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Fabrication, characterization and photocatalytic properties of CdS nanoparticles modiﬁed by N-doped TiO2 NTs

Gao D., Wang C., Jian Y., Li W., Dong P.

Materials Science Poland

2018

Vol. 36, No. 3

348--353

Highly ordered TiO2 nanotube arrays (TiO2 NTs) were prepared by anodic oxidizing method on a surface of Ti substrate. Fabrication of nitrogen-doped TiO2 nanotube arrays (N-TiO2 NTs) was carried out by immersion in ammonia solution. CdS nanoparticles loaded N-doped TiO2 nanotube arrays (CdS/N-TiO2 NTs) were obtained by successive ionic layer adsorption and reaction (SILAR) technique. The samples were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), photoluminescence (PL) emission spectra and ultraviolet-visible (UV-Vis) diffuse reflectance spectroscopy (DRS). The results indicate that the TiO2 nanotube diameter and wall thickness are 100 nm to 120 nm and 20 nm to 30 nm, respectively. Moreover, the morphology and structure of the highly ordered TiO2 NTs are not affected by N-doping. Furthermore, CdS nanoparticles are evenly distributed on the surface of TiO2 NTs. Finally, the photocatalytic activity of CdS/N-TiO2 NTs was evaluated by degradation of MO under visible-light irradiation. Compared with TiO2 NTs, N-TiO2 NTs, CdS/N-TiO2 NTs exhibited enhanced photocatalytic properties, and the highest degradation rate of CdS/N-TiO2NTs could reach 97.6 % after 90 min of irradiation.

Analysis of the start-up of natural bio-film colonization of constructed rapid infiltration system

Xu W., Yang J., Wang J., Jian Y., Tang M.

Polish Maritime Research

2016

S 1

32--35

Abstract: this paper studied the start-up of natural bio-film colonization under the conditions where wet-to-dry ratio was 1:6, hydraulic load was 0.8m3/m2·d, and water temperature was 100C-150C, it took 25d in total to become mature, after the success of bio-film colonization, the removal rate of COD and NH4+-N can be stabilized at 80%, and the removal rate of NH4+-N can reach 90% above. The microorganism was divided into the following stages during bio-film colonization:1. Reversible adhesion of cell on the surface of the carrier, 2.Irreversible adhesion of cell on the surface of the carrier, 3.Division of cell adhering to the surface of the carrier and formation of microcolony adhering to the surface of the carrier, 4.Growth of microcolony adhering to the surface of the carrier to be mature bio-film with three-dimensional structure. The process of natural bio-film colonization can be judged comprehensively according to removal rate of NH4+-N and COD, effluent pH as well as color of microbial film.