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The tribological characteristics of zirconium diboride particle reinforced composites processed by SPS

Sulima Iwona, Hyjek Paweł

Composites Theory and Practice

2024

R. 24, nr 1

2--8

The tribological properties of composites based on 316L steel reinforced with zirconium diboride (5 and 10 wt.%) were described. The composites were fabricated by the spark plasma sintering (SPS) method. Wear resistance tests were carried out using the ball-on-disc method at room temperature under dry friction conditions. Countersamples made of SiC, Si3N4, ZrO2 and AISI52100 steel were used in the tests. The determined parameters included the coefficient of friction μ, mass loss m and specific wear rate Ws(disc). After the tribological tests, the surfaces of the samples were examined under a confocal microscope. The obtained research results showed that the tribological properties depend on the test conditions (the type of countersample) and on the content of the ZrB2 reinforcing phase.

Przedstawiono właściwości tribologiczne kompozytow na osnowie stali 316L wzmocnionych diborkiem cyrkonu (5 i 10% wag.). Kompozyty zostały wytworzone z zastosowaniem metody Spark Plasma Sintering (SPS). Badania odporności na zużycie przeprowadzono, wykorzystując metodę ball-on-disc w temperaturze pokojowej w warunkach tarcia suchego. Testy przeprowadzono, stosując następujące przeciwprobki: SiC, Si3N4, ZrO2 i stal AISI52100. Wyznaczono współczynnik tarcia μ, ubytek masy m i wskaźnik zużycia Ws(disc). Powierzchnie probek po testach tribologicznych obserwowano za pomocą mikroskopu konfokalnego. Uzyskane wyniki badań wykazały, że właściwości tribologiczne zależą od warunkow badań (rodzaju przeciwprobki) i ilość fazy wzmacnianej ZrB2.

Evaluation of the corrosion resistance of spark plasma sintered stainless steel 316L matrix composites with zirconium diboride in sulfuric acid

Stępień Michał, Sulima Iwona, Hyjek Paweł, Kowalik Remigiusz

Archives of Civil and Mechanical Engineering

2022

Vol. 22, no. 3

art. no. e127

The infuence of the zirconium diboride content and the method of initial material preparation on the corrosion properties of the composite on the 316L stainless steel matrix were determined. The powders were prepared in a Turbula mixer and a planetary mill. The corrosion properties were estimated on the basis of electrochemical tests, including open-circuit potential measurement, potentiodynamic polarization, and electrochemical impedance spectroscopy. The presence of the ceramic phase changes the corrosion resistance of the tested materials due to porosity, which afects the corrosion mechanism. The standard potentiodynamic tests do not reveal poor corrosion resistance of porous materials, and only 24 h tests reveal accurate corrosion resistance of composite materials. Composites cannot go into a stable passive state because of the penetration of electrolytes into the pores and tend to oxidize systematically. 24-h corrosion tests indicate that samples prepared in a planetary mill show better corrosion resistance than those prepared in a Turbula mixer.