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Analysis of metal surfaces coated with europium-doped titanium dioxide by laser induced breakdown spectroscopy

Głogocka D., Noculak A., Pucińska J., Jopek W., Podbielska H., Langner M., Przybyło M.

Acta of Bioengineering and Biomechanics

2015

Vol. 17, no. 3

33--40

The surface passivation with titanium sol-gel coatings is a frequently used technique to control the adsorption of selected biological macromolecules and to reduce the exposure of the bulk material to biological matter. Due to the increasing number of new coating-preparation methods and new gel compositions with various types of additives, the quality and homogeneity determination of the surface covering is a critical factor affecting performance of any implanted material. While coating thickness is easy to determine, the homogeneity of the surface distribution of coating materials requires more elaborate methodologies. In the paper, the laser induced breakdown spectroscopy (LIBS) based method, capable to quantitate the homogeneity and uniformity of the europium in titanium dioxide sol-gel coatings on stainless steel surfaces prepared with two different procedures: spin-coating and dip-coating, is presented. The emission intensity of titanium has been used to determine the coating thickness whereas the relative values of europium and titanium emission intensities provide data on the coating homogeneity. The obtained results show that the spin-coating technique provides better surface coverage with titanium dioxide. However, when the surface coating compositions were compared the dip-coating technique was more reliable.

The study of properties TiAl-Nb alloys

Juřica J., Losertová M., Petlák D.

Zeszyty Naukowe. Mechanika / Politechnika Opolska

2010

z. 97

8-8

Subject of this work is an intermetallic alloy based on TiAl and doped with Nb with high creep resistance and good mechanical properties. The experimental Ti-Al-Nb material with two compositions of Ti-45Al-10Nb and Ti-40Al-15Nb was prepared from master alloy TiNb (55/45 wt. %) and Al pieces by plasma melting, vacuum induction remelting and casting into the rod shape. The samples were homogenisation annealed at 1100°C for 12 hours in Ar atmosphere and water quenched from 700°C. Heat treatment at 700 °C for 8 hours in Ar atmosphere as well as in hydrogen flowing gas was realised to prepare experimental material for hydrogen effect study. Microstructure of the specimens was studied by light and scanning electron microscopies, microhardness measurement and phase microanalysis were performed. The lamellar microstructure of the samples in as-cast and heat treated conditions formed of the ? (45 at.% Al) and ?2 (41 at.% Al) phases resulted from metallographic observation and EDS phase analysis. Microhardness values of the samples decreased after annealing and quenching. Effect of hydrogen on lamellar microstructure and microhardness values was studied on the hydrogen-charged and hydrogen-free specimens. X-ray diffraction analyses were performed on Ti-Al-Nb specimens.