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Physical and technological preconditions of melting-crystallisation temperature stabilisation

Prokhorenko V., Prokhorenko S., Mudry S., Bylica A.

Archives of Materials Science and Engineering

2008

Vol. 32, nr 1

29-32

Purpose: The precise temperature measurements need the using of temperature reference points - "temperature fixpoints" (TFP). The increase of measuring temperature interval and other reasons require of new TFP with high stability in different working conditions. On that reason the studying of liquid metals and metallic eutectic alloys has been carried out in this work. Design/methodology/approach: For experimental studies the physical properties measurements were used. Findings: Non-reproducibility of temperature fixpoints exist due to some reasons: no accounting the structural - thermodynamic state of melt; mass-heat processes are not enough taken into account. It is fixed, that the temperature fluctuations (and non-stability of crystallization plateau) are of two types: small fluctuations (up to (1-2) mK) are caused by phases (stages) of crystallization process; major fluctuations (at us: ±0,2K) crystallizations are caused convectional streams at the front. Fluctuations can be essentially reduced by approach to requirements of thermodynamic balance, but their complete elimination - is problematic. Research limitations/implications: The main parameters obtained from them are analysed. It is shown that melting-crystallization phase transition is influenced by structural state of melt and cooling condition. Practical implications: The results obtained here can be used in analysis of errors at high-precision temperature measurements and constructing of new temperature measuring and holding systems of high stability. Originality/value: The results of this study can be useful for researches in field of metrology, material science and physics of metals.

Advanced Materials & Technologies in Precisive Temperature Measurements

Prokhorenko S., Mudry S., Panas A. J., Stadnyk B, Kowalczyk A.

Pomiary Automatyka Kontrola

2006

R. 52, nr 12

4-6

The studies of eutectic melts Cd-Sn, Bi-Cd are carried out be means of X-ray diffraction, metallography and differential scanning calorymetry methods in order to check the possibility to use them as temperature fix-point. It is shown that outside energetic influence on melt can change some parameters of structure and physical properties.

Stopy eutektyczne Cd-Sn, Bi-Cd badane były metodami dyfrakcji rentgenowskiej, metalografii oraz różniczkowej kalorymetrii skaningowej w celu uzyskania wiedzy o możliwości używania ich jako temperaturowych punktów odniesienia. Wykazano, że zewnętrzna obróbka energetyczna stopów zmienia ich parametry strukturalne i właściwości fizyczne.