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1 Polish Journal of Applied Chemistry

1 2008

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Synthesis and transformation of 4-difluoromethylsulfonyl-2-nitrophenylsulfenyl chloride into new compounds with promising pesticidal activity

Ochal Z., Trojanowska A.

Polish Journal of Applied Chemistry

2008

Vol. 52, nr 3-4

131-138

The synthesis of 4-difluoromethylsulfonyl-2-nitrophenylsulfenyl chloride and its transformation into new compounds with potential pesticidal activity is reported. The title compound was obtained by three step synthesis starting from 4-difluoromethylchlorophenyl sulfone. It was nitrated and then subjected to the SNAr reaction with sodium disulfide to give proper diphenyl disulfide which was chlorinated by chlorine. Obtained phenylsulfenyl chloride was transformed into sulfonamide derivatives by reactions with amines.