The Co-Ni-Mo alloy powders were electrochemically deposited from alkaline ammonical electrolyte containing two or three different elements, Co, Ni and/or Mo at a constant current density. The obtained Co-Ni-M powders were studied using EDS, XRay and SEM analysis. Based on the obtained experimental results it can be concluded that by appropriate selection of chemical composition of the electrolyte for deposition, varying of Co, Ni and Mo ions ratios and current density it can be influenced on the particle sizes of deposited powders. X-ray results suggest that the obtained powders have amorphous structure.
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