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Mechanism of Ca2+/Fe3+-based synergistic activation of quartz

Liu Rongxiang, Yang Zhanfeng, Li Jie, Li Qiang, Wang Zhenjiang, Luo Xiaofeng

Physicochemical Problems of Mineral Processing

2023

Vol. 59, iss. 1

art. no. 162262

Although the flotation behaviors of iron concentrate and quartz are significantly different, quartz is the primary factor that affects the quality of iron concentrate. The flotation mechanism of quartz in the presence of mixed cationic Ca2+/Fe3+-co-activated SDS catcher was studied by conducting flotation tests with pure quartz mineral. The solution chemical calculation method, zeta potential calculation method, Fourier transform infrared (FT-IR) spectroscopy technique, X-ray photoelectron spectroscopy (XPS) technique, and other techniques were used to conduct the studies. The results showed that the maximum Ca2+/Fe3+-based synergistic activation of the flotation recovery process could be achieved in a certain range of pH values when three different activators were added sequentially. Analysis of the zeta potential values revealed that the Ca2+/Fe3+-activated quartz surface improved the extent of positive electricity generated and enhanced the SDS adsorption ability of the quartz surface. Results obtained using the FT-IR technique revealed that Ca2+/Fe3+ exerted a synergistic effect, and the adsorption process exploited the single oxygen bond interactions in the monovalent hydroxyl complex Ca(OH)+ and the double oxygen bond interactions in the Fe(OH)3 precipitates. Results obtained using the XPS technique revealed that the synergistic effect exerted by Ca2+/Fe3+ was significantly stronger than that exerted by Ca2+ or Fe3+ alone. The stable Fe-based six-membered chelate ring was formed on the surface of quartz when Fe3+ was the activator, and the chain-like Ca-based complex was formed when Ca2+ was the activator. The adsorption process on the surface of quartz proceeded following chemical as well as physical adsorption pathways. The results revealed that Ca(OH)+ and Fe(OH)3 played prominent roles during the activation of quartz surfaces in the presence of Ca2+/Fe3+.

Phase Behavior and Solubilization of Microemulsion System Formed by Aliphatic Polyethenoxy Ether and Sodium Dodecyl Sulfonate

Chen J. F., Gao Y. Ch., Li H. L., Chai J. L., Yang X. D., Qin C. K.

Polish Journal of Chemistry

2008

Vol. 82, nr 5

1067-1076

The phase behavior and solubilization of the quaternary system AEO-9/AS/n- butanol /alkane/NaCl solution were investigated with delta-gamma and epsilon-beta fishlike phase diagrams. Two kinds of diagrams were plotted and compared in their shapes, HLB plane equations and solubilization power representations. Their HLB plane equations were used to calculate the composition of the hydrophile-lipophile balanced interfacial layer. It is found that the synergism between AEO-9 and AS in the inter facial layer in solubilization power exists. The influences of oil and aqueous medium on the epsilon-beta fishlike phase diagram were also discussed.