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Mathematical forecasting composition of secondary carbides in the single-crystal superalloys

Glotka O.A., Olshanetskii V.I.

Archives of Materials Science and Engineering

2021

Vol. 111, nr 1

34--41

Purpose: Predicting the specifics of the distribution of alloying elements between secondary carbides, their topology, and morphology, as well as the composition for a single-crystal multicomponent system of the type Ni-11.5Cr-5Co-3.6Al-4.5Ti-7W-0.8Mo-0.06C using the calculated CALPHAD (passive experiment) versus scanning electron microscopy (active experiment). Design/methodology/approach: This work presents the results of studies of the distribution of chemical elements in the composition of carbides, depending on their content in the system. The studies were carried out using an electron microscope with computer analysis of images and chemical composition. Findings: It was found that the influence of alloying elements on the composition of carbides is complex and is described by complex dependencies that correlate well with the obtained experimental results. Research limitations/implications: An essential problem is the prediction of the structure and properties of superalloys without or with a minimum number of experiments. Practical implications: The obtained dependencies can be used both for designing new superalloys and for improving the compositions of industrial alloys. Originality/value: The value of this work is that the obtained dependences of the influence of alloying elements on the dissolution (precipitation) temperatures and the distribution of elements in secondary carbides in the superalloy of the Ni-11.5Cr-5Co-3.6Al-4.5Ti-7W- 0.8Mo-0.06C system. It was found that changes in the course of the curves of temperature dependence on the element content closely correlate with thermodynamic processes occurring in the system, that is, the curves exhibit extrema accompanying the change in the stoichiometry of carbides or the precipitation of new phases.

Experimental study on fabricating micro-holes in DD5 single-crystal nickel-based superalloy using electrical discharge drilling

Gong Siqian, Sun Yao, Jin Liya, Su Zhipeng

Archives of Civil and Mechanical Engineering

2020

Vol. 20, no. 3

337--352

The single-crystal superalloy materials have been rapidly developed and widely used in advanced thermal structural components due to their excellent comprehensive physical and chemical properties under high-temperature service conditions. However, conventional micro-hole making results in defects such as edge breakage and burr. In this study, the electrical discharge drilling (EDD) combined with helical microelectrode is first adopted to fabricate DD5 single-crystal nickel-based superalloy. The effects of tool geometry and machining parameters on subsurface damage layer, micro-hole taper, surface morphology, surface roughness and machining time were investigated in detail. Experimental results indicated that helical microelectrode can obtained smoother surface without debris deposition and thinner subsurface damage layer depth lack of micro-cracks compared with cylindrical microelectrodes. Additionally, the computational fluid dynamics model was developed to analyze working fluid movement and reveal effective debris removal mechanism of helical microelectrode. The vortices will be generated in lateral gap fluid between micro-hole and helical microelectrode and have a certain delay time. The surface roughness and dimensional precision of micro-holes fabricated by helical microelectrodes are greatly improved and machining efficiency is also improved by 30.94% compared to cylindrical microelectrodes. This work could provide theoretical and process guidance to assist in realizing high surface quality and low subsurface damage of micro-holes obtained with EDD process.