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Removal of Sesame Oil from Artificial Wastewater Applying Fenton Process and Comparing It with Actual Wastewater

Nasir Mohsin J., Kadhum Zaid F., Kariem Nagham O., Jasim Zaid M.

Journal of Ecological Engineering

2022

Vol. 23, nr 10

248--254

In this research the removal of sesame oil from aritifical water by Fenton process technique was investigated. The results of removal efficiency were compared with actual wastewater. Effect of time, pH, mixing speed, temperature, oil content were investigated to find the perfect circumstances. The conducted experiments revealed that the optimal conditions for this process were 160 minutes of reaction time in an acidic medium where pH was equal to 3.5, temperature was discovered to be 25 °C, the optimal mixing speed was at 500 rpm, and the Sesame oil concentration amounted to 1500 mg/l. Applying the optimal conditions for this processing, the results of compersion showed the sesame oil had a removal efficiency of 95% for the artificial wastewater in which the concentration decreased from 12800 to 68 mg/l, while the Fenton method was used to treat an actual sample of wastewater the removal efficiency is found to be 87%.

Technological parameters of epoxidation of sesame oil with performic acid

Musik M., Milchert E., Malarczyk-Matusiak K.

Polish Journal of Chemical Technology

2018

Vol. 20, nr 3

53--59

The course of epoxidation of sesame oil (SO) with performic acid formed „in situ” by the reaction of 30 wt% hydrogen peroxide and formic acid in the presence of sulfuric acid(VI) as a catalyst was studied. The most advantageous of the technological independent parameters of epoxidation are as follows: temperature 80°C, H2O2 C=C 3.5:1, HCOOH/C=C 0.8:1, amount of catalyst as H2SO4 /(H2O2 +HCOOH) 1 wt%, stirring speed at least 700 rpm, reaction time 6 h. The iodine number (IN), epoxy number (EN), a relative conversion to oxirane (RCO) and oxirane oxygen content (EOe) were determined every hour during the reaction. Under optimal conditions the sesame oil conversion amounted to 90.7%, the selectivity of transformation to epoxidized sesame oil was equal to 93.2%, EN = 0.34 mol/100 g, IN = 0.04 mol/100 g oil (10.2 g/100 g oil), a relative conversion to oxirane RCO = 84.6%, and oxirane oxygen content of EOe = 5.5%.