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Microstructure characterization of welds in X5CrNiCuNb16-4 steel in overaged condition

Ziewiec A., Zielińska-Lipiec A., Kowalska J., Ziewiec K.

Advances in Materials Science

2019

Vol. 19, nr 1(59)

57--69

The paper presents the results of the investigation of microstructure of the welded X5CrNiCuNb16-4 (17-4PH) steel after solution treatment and aging at 620°C for different periods. The microstructure and the phase composition of the steel was investigated using light microscopy (LM), scanning electron microscopy (SEM), energy dispersive spectrometry (EDS), transmission electron microscopy (TEM) and the X-ray diffraction (XRD). Hardness was measured for samples aged at different times. Density distributions of Cu precipitates were established. The investigation has shown that the microstructure of the X5CrNiCuNb16-4 steel welds after aging at 620 ° C consists of tempered martensite, fine Cu precipitates and austenite. It was observed that the size of the Cu precipitates increases with increasing the aging time, what affects the decrease of hardness. Simultaneously, the quantity of reversed austenite increases with increase of aging time. It was revealed that enrichment of the austenite in Ni, Cu and C affects the increase of Ms, but this factor does not determine the stability of austenite.

Zastosowanie MFM do opisu struktury warstw azotowanych jarzeniowo na stali Fe27Ni2TiAlMoNb

Borowski T., Jeleńkowski J., Wierzchoń T.

Inżynieria Materiałowa

2010

Vol. 31, nr 1

23-26

W artykule scharakteryzowano właściwości magnetyczne i stabilność austenitu, martenzytu atermicznego i odkształceniowego stali Fe27Ni2TiAlMoNb a także austenitu azotowego (fazy S o rożnych stałych sieciowych), który tworzy się w czasie azotowania jarzeniowego poniżej temperatury As. Morfologi i analizę składników strukturalnych, tworzących się w procesie azotowania jarzeniowego, opisano, stosując mikroskop sił magnetycznych MFM, a do określenia składu fazowego wytworzonych warstw azotowanych zastosowano dyfraktometr rentgenowski.

The paper analyzes the magnetic properties and stability of austenite, athermal martensite, and deformation martensite that form in Fe27Ni2TiAlMoNb steel subjected to glow discharge assisted nitriding, and also of nitrogen austenite (S phase with various lattice constants) which occurs when the nitriding process is conducted below the temperature As. The analysis of these structural components and their morphology was performed using a magnetic force microscope (MFM), whereas the phase composition of the nitrided layers produced on this steel was determined by X-ray diffraction.