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Phase Evolution During Extraction and Recovery of Pure Nd from Magnet

Rasheed Mohammad Zarar, Nam Sun-Woo, Lee Sang-Hoon, Park Sang-Min, Cho Ju-Young, Kim Taek-Soo

Archives of Metallurgy and Materials

2021

Vol. 66, iss. 4

1001--1005

Liquid Metal Extraction process using molten Mg was carried out to obtain Nd-Mg alloys from Nd based permanent magnets at 900°C for 24 h. with a magnet to magnesium mass ratio of 1:10. Nd was successfully extracted from magnet into Mg resulting in ~4 wt.% Nd-Mg alloy. Nd was recovered from the obtained Nd-Mg alloys based on the difference in their vapor pressures using vacuum distillation. Vacuum distillation experiments were carried out at 800°C under vacuum of 2.67 Pa at various times for the recovery of high purity Nd. Nd having a purity of more than 99% was recovered at distillation time of 120 min and above. The phase transformations of the Nd-Mg alloy during the process, from Mg12Nd to α-Nd, were confirmed as per the phase diagram at different distillation times. Pure Nd was recovered as a result of two step recycling process; Liquid Metal Extraction followed by Vacuum Distillation.