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Investigation of structural-geometric parameters and elemental composition of spherical VT20 alloy powders

Duriagina Z. A., Filimonov O. S., Kulyk V. V., Lemishka I. A., Kuziola R.

Journal of Achievements in Materials and Manufacturing Engineering

2019

Vol. 95, nr 2

49--56

Purpose: Identification of structural-geometrical parameters, technological properties and elemental composition of spherical powders in a wide fraction range with respect to the VT20 alloy has been carried out. This is important for evaluating the optimum filling of a given volume by mixture of powders of different fractions during 3D printing. Design/methodology/approach: During the investigation of spherical Ti-alloy powders, a comprehensive approach was performed using Scanning Electron Microscopy (SEM), Energy-Dispersive X-ray Spectroscopy (EDS), Dynamic Light Scattering (DLS) and Inductively Coupled Plasma Mass Spectrometry (ICP-MS). The surface morphology of the powders was studied on a Tuescan Vega 3 Scanning Electron Microscope. Using the Quantax energy dispersive spectrometer, element distribution maps were obtained and histograms of element distribution in the investigated powders were constructed. ICP-MS analysis was performed to clarify the elemental composition. DLS analysis using Malvern's Zetasizer Nano-ZS equipment allowed us to determine the functional parameters (hydrodynamic radius – Rh, zeta potential – z and specific conductivity) of particles of titanium alloy powder that indirectly indicate a tendency to form conglomerates. Findings: According to the microscopic examinations, the VT20 alloy powder consists of globular-shaped particles with the lamellar traces on their surfaces. The uniformity of the chemical element distribution within each fraction of the investigated powders was confirmed by EDS, and the full conformity of the powder fractions with the elemental composition of the VT20 alloy was confirmed by ICP-MS. The DLS method allowed to establish that the formation of conglomerates would not occur within the studied fractions of the VT20 alloy powder. Research limitations/implications: The use of high sensitive investigation methods gives understanding of the mechanisms of fine structure formation and possibility to control the processes of powder coagulation in the stage of electrostatic interactions. Practical implications: The obtained results can be used for the formation of fine spherical particles of the powder, but at the same time, these technologies can be extended for the particles of non-spherical shape. Originality/value: The DLS method allowed to establish that the formation of conglomerates would not occur within the studied fractions of the VT20 alloy powder. This, in turn, will improve powder melting during 3D printing. The measured zeta potential values allowed us to reveal mechanisms of fine structure formation and to control the processes of powder coagulation in the stage of electrostatic interactions.

Badania emulsji adiuwantów metodą dynamicznego rozpraszania światła

Włodarczyk M., Włodarczyk A., Wybieralski J.

Ekologia i Technika

2006

R. 14, nr 2

48-52

W pracy wykonano wstępne badania metodą dynamicznego (DLS) rozpraszania światła eksperymentalnych wodnych roztworów adiuwantu Break-Thru S 240. Wszystkie pomiary wykonano w Zakładzie Biofizyki Molekularnej A. Mickiewicza w Poznaniu. Wstępne badania roztworów adiuwantu metodą DLS wskazują na polidyspersję badanych układów.

The paper present results of a preliminary study of adjuvant Break-Thru S 240 experimental water solutions by Dynamic Light Scattering method. All measurements have been done at the Biophysics Department, Adam Mickiewicz University in Poznan.