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Luminescence chronostratigraphy for the loess deposits in Złota, Poland

Moska P., Adamiec G., Jary Z., Bluszcz A., Poręba G., Piotrowska N., Krawczyk M., Skurzyński J.

Geochronometria

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2018

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Vol. 45, no. 1

44--55

EN

Loess formations in Poland display a close relationship with cooling and warming trends of the Northern Hemisphere during the Pleistocene. Loess sequences sensitively record regional palaeoclimatic and palaeoecological changes. The Złota loess profile (21°39’E, 50°39’N) provides a unique opportunity to reconstruct climate conditions in the past in this part of Poland. This continuous sequence of loess and palaeosol deposits allows to distinguish between warmer and more humid climate which is favourable for soil development and much colder and dry periods which are conducive to loess accumulation. The silty and sandy aeolian material originates mainly from weathered rock surfaces affected by frost shattering or from glaciofluvial/fluvial deposits of river flood plains. In Poland, loess and loess-like formations occur in the southern part of the country, mostly in the south polish uplands, i.e. in the Lublin, Sandomierz, and Cracow Uplands. We used different techniques to establish a chronological framework for this site. 21 samples for luminescence dating were collected from the investigated loess profile in Złota. Infrared post-IR IRSL dating method was applied to the polymineral fine grains (4–11µm). The dating results are accompanied by detailed analyses of the geochemical composition, organic carbon and carbonate. Also, analysis of magnetic susceptibility and grain-size distribution were investigated. Based on such a large stratigraphic dataset an age-depth model using OxCal has also been constructed for this site.

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Luminescence Dating of Fluvial Deposits in the Rock Shelter of Cueva Antón, Spain

Burow Ch., Kehl M., Hilgers A., Weniger G. - Ch., Angelucci D. E., Villaverde V., Zapata J., Zilhão J.

Geochronometria

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2015

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Vol. 42, no.1

107--125

EN

The fluvial sediments at Cueva Antón, a Middle Palaeolithic rock shelter located in the valley of the River Mula (Southeast Spain), produced abundant lithic assemblages of Mousterian affinities. Radiocarbon dates are available for the upper part of the archaeological succession, while for the middle to lower parts chronometric data have been missing. Here we present luminescence dating results for these parts of the succession. Quartz OSL on small aliquots and single grain measurements yield ages ranging from 69 ± 7 ka to 82 ± 8 ka with a weighted mean of 72 ± 4 ka for sub-complexes AS2 to AS5. Equivalent dose estimates from large aliquots were highest and inconsistent with those from single grains and small multiple grain aliquots. This is probably caused by the presence of oversaturating grains, which have been quantified by single grain measurements. Additional post-IR IRSL measurements on coarse grained feldspar give strong support to a well-bleached quartz OSL signal. While independent chronometric control is missing, the results are within the expected age range and support the notion of a rapid accumulation of the fluvial deposits.

3

The D e (T, t) plot: A straightforward self-diagnose tool for post-IR IRSL dating procedures

Fu X.

Geochronometria

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2014

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Vol. 41, no. 4

315--326

EN

This study presents a new self-diagnose method for the recently developed post-IR infrared stimulated luminescence (pIRIR) dating protocols. This criterion studies the dependence of equivalent dose (D e) on measurement-temperature (T) and time (t), by applying the D e (t) analysis to the IRLS and pIRIR signals measured under different temperatures, and combines these D e (t) plots into one, so-called the D e (T, t) plot. The pattern of the D e (T, t) plot is shown to be affected by anomalous fading, partial bleaching and non-bleachable signal. A D e plateau can be achieved in the D e (T, t) plot only when the effects of these factors are insignificant. Therefore, this plot can be used as a self-diagnose tool for the validity of pIRIR results. The D e (T, t) analysis has been applied to four recently developed pIRIR protocols, using aeolian samples with different ages. The results show that this self-diagnose tool can be applied to different pIRIR protocols for validating the pIRIR dating results and evaluating the pIRIR measurement conditions.

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Review and assessment of the potential of post-IR IRSL dating methods to circumvent the problem of anomalous fading in feldspar luminescence

Li B., Jacobs Z., Roberts R. G., Li S.-H.

Geochronometria

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2014

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Vol. 41, no. 3

178--201

EN

Quartz has been the main mineral used for optically stimulated luminescence (OSL) dating of sediments over the last decade. The quartz OSL signal, however, has been shown to saturate at rel-atively low doses of ~200–400 Gy, making it difficult to be used for dating beyond about 200 thou-sand years (ka), unless the environmental dose rate is low. The infrared stimulated luminescence (IRSL) from feldspars has been shown to continue to grow to higher dose levels than quartz OSL. The application of IRSL dating of feldspars, however, has long been hampered by the anomalous fading effect. Recent progress in understanding anomalous fading of the infrared stimulated luminescence (IRSL) signals in potassium-feldspar has led to the development of post-IR IRSL (pIRIR) protocols and also a multiple elevated temperature (MET) stimulation (MET-pIRIR) protocol. These procedures have raised the prospect of isolating a non-fading IRSL component for dating Quaternary deposits containing feldspars. In this study, we review the recent progress made on (1) overcoming anomalous fading of feldspar, and (2) the development of pIRIR dating techniques for feldspar. The potential and problems associated with these methods are discussed.

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Comparing different post-IR IRSL approaches for the dating of Holocene coastal foredunes from Ruhnu Island, Estonia

Preusser F., Muru M., Rosentau A.

Geochronometria

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2014

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Vol. 41, no. 4

342--351

EN

Different post-IR Infrared Stimulated Luminescence (IRSL) approaches are applied to sediments from a Holocene coastal foredune sequence on Ruhnu Island in the eastern Baltic Sea. The comparison of D e-values and ages determined by the different approaches is complimented by fading and bleaching experiments. The fading experiments imply strong fading of IRSL (50°C) signals and no fading of any of the post-IR IRSL signals, but this is not confirmed by the determined D e-values. In fact, post-IR IRSL (150°C) D e-values agree within errors with those calculated for IRSL (50°C). From the bleaching experiments it is inferred that the higher values observed for post-IR IRSL at more elevated stimulation temperatures (225°C/290°C) are likely related to either thermal transfer and/or slow-to-bleach components within the signal. For the dating of the Holocene foredune sequence of Ruhnu Island, the post-IR IRSL (150°C) approach is preferred and these agree with the limited independent age control available from radiocarbon dating. Accordingly, the sequence formed between ca. 7.0 ka and 2.5 ka ago.

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Luminescence dating of volcanogenic outburst flood sediments from Aso volcano and tephric loess deposits, southwest Japan

Tsukamoto S., Kataoka K. S., Miyabuchi Y.

Geochronometria

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2013

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Vol. 40, no. 4

294--303

EN

Luminescence dating has been applied to volcanogenic outburst flood sediments (Takuma gravel bed) from Aso volcano, Japan, and tephric loess deposits overlying the gravel bed. The poly-mineral fine grains (4-11 μm) from loess deposits were measured with pulsed optically stimulated luminescence (pulsed OSL) and post-IR infrared stimulated luminescence (pIRIR) methods, whereas the Takuma gravel bed containing no quartz, was measured with IRSL and pIRIR methods using sand sized (150-200 μm) plagioclase. The loess deposits date back at least to ~50 ka by consistent IRSL, pIRIR and pulsed OSL ages from the lowermost part of the loess deposits from one section. The ages obtained from the bottom part of the other loess section are not consistent each other. However, we consider that the pIRIR age (72±6 ka) which showed negligible anomalous fading is most reliable, and regard as a preliminary minimum age of the Takuma gravel bed. The equivalent doses (De) for the plagioclase from the Takuma gravel bed have a narrow distribution and the weighted mean of the three samples yield an age of 89±3 ka. This age is in agreement with the last caldera-forming eruption of Aso volcano (~87 ka) and it is likely that the pIRIR signal has not been bleached before the deposi-tion. IRSL dating without applying pIRIR using small aliquots was also conducted, however, the IRSL signal shows no clear evidence of an additional bleaching during the event of outburst flood from the caldera lake.

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Stability of IRSL signals from sedimentary K-feldspar samples

Thomsen K. J., Murray A. S., Mayank J.

Geochronometria

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2011

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Vol. 38, no. 1

1-13

EN

Recent work has identified IR stimulated luminescence signals at elevated temperature from both potassium- and sodium-rich feldspars that have much lower anomalous fading rates than the conventional signal measured using IR stimulation at 50°C. This paper examines the stability of these signals for potassium-rich sedimentary feldspars. We show that the natural post-IR IRSL (pIRIR) signal from a 3.6 Ma old sample is in apparent saturation on a laboratory generated dose response curve, i.e. it does not show detectable fading in nature although a low fading rate is observed on laboratory time scales. We show that the pIRIR signal has a greater thermal stability than the IRSL signal and that the trend in increasing thermal stability is mirrored by a decreasing fading rate. We also investigate the effect of preheat temperature and IR stimulation power on the decay shape and conclude that the data can be explained in terms of either a single- or multiple-trap model. We present evidence that may suggest that at least part of pIRIR signal is derived from a high temperature trap (~550°C thermoluminescence (TL) peak), although again the data can also be explained in terms of a single-trap model. Finally, we present dose response curves and characteristic curvature constants (D0) values for various IRSL signals and conclude that the more stable signals saturate more quickly than the less stable signals and that the initial and final signals saturate at approximately the same level.

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IRSL and post-IR IRSL residual doses recorded in modern dust samples from the Chinese loess plateau

Buylaert J.-P., Thiel Ch., Murray A. S., Vandenberghe D. A. G., Yi S., Lu H.

Geochronometria

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2011

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Vol. 38, no. 4

432-440

EN

Using a set of modern/young (0 to about 200 years old) dust samples collected from the Chinese Loess Plateau the bleachability of IRSL measured at 50°C (IR50) and post-IR50 elevated temperature IRSL (measured at 225°C and at 290°C) is investigated by measuring the apparent (residual) doses recorded by these signals. Doses recorded by quartz OSL are used as a reference. Allowing for differences in dose rates it seems that both IRSL and post-IR IRSL signals yield residual doses that are significantly larger than the doses measured in quartz. These residual doses can be largely explained by thermal transfer caused by preheating. Nevertheless, we advise against the use of a low temperature preheat (<200°C) with IR50 to date loess samples because, as has been reported before, the signal appears to be thermally unstable. In general, we conclude that it may not be advisable to apply post-IR IRSL dating to Chinese loess samples where residuals of up to ~20 Gy are a significant fraction of the total dose. However, these residuals quickly become unimportant when dating older samples, and this is the age range in which post-IR IRSL dating is likely to be most useful.