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Core-shell SiO2/Ag composite spheres: synthesis, characterization and photocatalytic properties

Wu Z. G., Jia Y. R., Wang J., Guo Y., Gao J. F.

Materials Science Poland

2016

Vol. 34, No. 4

806--810

Core-shell SiO2/Ag composite spheres with dense, complete and nanoscaled silver shell were prepared by using a novel facile chemical reduction method without surface modification of silica at room temperature. The core-shell composites were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), UV-Vis spectroscopy and energy dispersive X-ray spectroscopy (EDX). The photocatalytic properties towards the degradation of methyl orange (Mo) of the prepared SiO2//Ag composites were also tested. The studies showed that the surface of SiO2/ microspheres was homogeneously and completely covered by Ag nanoparticles and the composite exhibited excellent photocatalytic activities. The possible reaction mechanisms for the formation of the silica-silver core-shell spheres were also discussed in this paper.

TiO2 supported on SiO2 photocatalysts prepared using ultrasonic-assisted sol-gel method

Yang X. L., Liu C. J., Liu Y. Q., Li X., Xu Y. H.

Materials Science Poland

2011

Vol. 29, No. 3

189--194

Guangdong TiO2-SiO2 (TiO2 supported on SiO2) photocatalysts were prepared using an ultrasonic-assisted sol-gel method. These photocatalysts were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR) and photoluminescence spectra (PL). Their photocatalytic activities were investigated by the method of methyl orange oxidation. It was found that the photocatalytic activity of TiO2-SiO2 was optimal when the molar ratio of hexadecyl trimethyl ammonium bromide to titanium butoxide was 1:10. The average crystallite size of TiO2-SiO2 was smaller than that prepared by the stirring method. Furthermore, for pure anatase phase samples, it was shown that the lower the photoluminescence intensity, the higher the photocatalytic activity.