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Application of the QuEChERS Method for the Analysis of Contamination by Pesticide Residues in the Sediments of Three Moroccan Lagoons

Fegrouche Rachida, Dahak Hicham, El Kamli Taha, Oussekour Mohammed, Zaza Saida, Ben Salem Abdelkrim, Benyacoub Badreddine

Journal of Ecological Engineering

2023

Vol. 24, nr 12

336--345

Agricultural, industrial, and domestic activities are major contributors to the contamination of natural environments. The aim of this study is to assess the level of sediment contamination by organic pollutants in three Moroccan lagoons: Moulay Bousselham, Oualidia, and Khnifiss. samples were analyzed using liquid chromatography (LC) coupled with mass spectrometry (MS) in Multiple Reaction Monitoring (MRM) mode to detect organophosphorus, carbamate, urea and its derivatives, and other chemical groups. Gas chromatography (GC) coupled with mass spectrometry (MS) was also used to analyze organochlorines. The samples were subjected to dispersive solid-phase extraction (dSPE) using QuEChERS before analysis. Fifteen active substances were detected, including organochlorines, organophosphates, carbamates, ureas, pyrethroids, and others. Three active substances, known for their high toxicity in aquatic environments (carbendazim, malathion, and chlorpyrifos), were identified. The heptachlor molecule (organochlorine family), although banned in Morocco, was still detected in the sediments of the lagoons of Oualidia and Khenifiss. Given the potential harm that these pesticides can cause to living organisms, it is crucial to introduce new crop protection techniques to address this issue.

Potencjał redox jako istotny parametr kontroli technologicznych procesów produkcji szkieł użytkowych. Cz. I - Potencjał redox stopu szklanego oraz czynniki wpływające na jego wartość.

Zawiła J.

Szkło i Ceramika

2006

R. 57, nr 3

14-19

In the paper, there have been described problems connected with function of the redox state in the melting process of the commercial glasses. Definition and the most important redox-reactions occuring during melting process of glass batch components have been presented as well as influence of some essential factors on the redox-potential values. Especially, attention has been devoted the problems connected with influence of such factors as chemical composition of glass batch, composition of gas atmosphere above the surface of the melt, application and organic contaminations of the cullet.