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Semi-organic nonlinear optical material: (((4-sulfonatophenyl)ammonio)oxy)zirconium for dielectric and photonics applications

Vinoth E., Vetrivel S., Gopinath S.

Materials Science Poland

2020

Vol. 38, No. 3

434--442

This article discusses the growth and characterization of (((4-sulfonatophenyl) ammonio)oxy) zirconium (SAOZ) single crystals. Sulphanilic acid incorporated zirconium oxychloride semi-organic single crystals have been synthesized by slow evaporation technique. From the X-ray studies, lattice parameters a = 7.31 Å, b = 7.51 Å, c = 13.92 Å, volume = 765 Å3 have been found and so the crystal has been identified as orthorhombic with non-centrosymmetric space group P212121. The powder XRD examination demonstrated the quality and high crystalline nature of the grown crystal. The presence of functional groups was confirmed by FT-IR technique. The chemical structure of the compound was established by 1H and 13C NMR spectra. The optical transmittance window and the low cutoff wavelength of SAOZ have been identified by UV-Vis-NIR studies. Photoluminescence studies showed a wide blue light emission. TG and DTA examinations were carried out to characterize the thermal behavior of the grown crystal. The mechanical strength of the grown crystal was analyzed by the Vickers microhardness test. The elemental analysis was done by EDAX. The dielectric response of the crystals was analyzed in the frequency range of 50 Hz to 5 MHz at various temperatures and the outcomes were discussed. The SHG efficiency was estimated in correlation with KDP by employing powder Kurtz method.

Research od compound Nd: YAG phase-conjugate resonator with stimulated Brillouin scattering (SBS) cell

Qu J., Zhang W., Gao X.

Optica Applicata

2005

Vol. 35, nr 1

42-46

How to improve the quality of output beam of phase conjungation cavity is a problem. In this paper, the output characteristic of compound phase-conjugate resonator with stimulated Brillouin scattering (SBS) cell was reported. The experimental results indicated it has high output energy and excellent stability. The output energy of the single pulse can reach 90 mJ, and the width of it is about 25ns. The results of pulse widths, output energies and beam profiles were given.