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Ocena jakości warstw wierzchnich nanometalicznych napawanych GMA w sposób zrobotyzowany na powierzchniach krzywek przesiewacza koksu ze stali Hardox 400

Lisiecki A., Kubica S., Ślizak D., Kurc-Lisiecka A.

Przegląd Spawalnictwa

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2015

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R. 87, nr 9

82--86

PL

Przedmiotem badań była analiza wpływu parametrów procesu zrobotyzowanego napawania GMA drutem rdzeniowym EnDOtec DO390N o średnicy 1,6 mm powierzchni roboczych krzywek przesiewacza koksu ze stali trudnościeralnej Hardox 400 na jakość, kształt i odporność na zużycie ścierne napoin. Próby technologiczne napawania prowadzono na stanowisku wyposażonym w robota spawalniczego Reis SRV6 oraz synergiczne urządzenie spawalnicze TotalArc 5000. Badania wykazały, iż napoiny próbne wykonane drutem rdzeniowym EnDOtec DO390N posiadają osnowę metaliczną na bazie żelaza z wydzieleniami węglików boru o znacznej dyspersji, równomiernie rozłożonymi w osnowie. Wielkość zarówno węglików boru, jak i niektórych składników fazowych nie przekracza 1,0 μm, a udział faz o tak niewielkiej wielkości w napoinie wynosi co najmniej 30 %, zależnie od parametrów napawania. W związku z tym napoiny próbne wykazują cechy materiału metalicznego nanostrukturalnego. Pomimo wysokiej twardości ok. 62 do 64 HRC, napoiny cechują się nieznacz- ną skłonnością do pękania w warunkach, w jakich prowadzono próby napawania zrobotyzowanego GMA. Badania odporność na zużycie ścierne typu metal-metal wykonane za pomocą próby ball-on-plate wykazały, że napoiny próbne posiadają prawie siedmiokrotnie wyższą odporność na zużycie w porównaniu do stali Hardox 400.

EN

The subject of the study was to analyse the influence of process parameters of robotic GMA cladding, by cored wire EnDOtec DO390N having a diameter of 1,6 mm, of cams working surfaces of coke screening plant made of Hardox 400 wear resistant steel on the quality, shape and abrasive wear resistance of test surface layers. The tests of cladding were performed by means of a welding robot Reis SRV6 and a synergic welding machine TotalArc 5000. The test surface layers produced by the cored wire EnDOtec DO390N have iron based metallic matrix with boron carbides precipitations with a large dispersion, evenly distributed in the matrix. The size of boron carbides and the size of some phase constituents do not exceed 1,0 μm, and the proportion of phase constituents of such a small size in the deposited surface layers is at least 30%, depending on the deposition parameters. Therefore, the deposited surface layers exhibit characteristics of nanostructured metallic material. Despite the high hardness of approx. 62 to 64 HRC, the deposit show just slight tendency to cracking, under the applied conditions of robotized GMA cladding. The abrasive resistance metal-metal wear investigations, conducted by means of ball-on-plate test showed that the test deposited surface layers have almost seven times higher wear resistance compared to Hardox 400 steel.

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Applications of newly developed nanostructural and microporous materials in biomedical, tissue and mechanical engineering

Dobrzański L. A.

Archives of Materials Science and Engineering

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2015

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Vol. 76, nr 2

53--114

EN

Purpose: The purpose of the paper is to present the main results of own research in 3 principal aspects indicating that the research is up to date and modern. This relates to nanotechnologies, modern biomedical materials and rapid manufacturing techniques used for the production of, in particular, microporous materials applied for medical and dental purposes. The paper comprises the explanation of structural mechanisms and phase transformations taking place in newly created engineering nanostructural and microporous materials under the influence of the applied, advanced technological processes newly developed, and especially nanotechnological processes, using the most modern scientific and research equipment being at disposal of modern materials engineering, in particular with the common use of high-resolution transmission electron microscopy (HRTEM). The results of investigations into the formation of the structure and surface properties results according to a different thickness scale of coatings or surface zone, from several hundred nanometres to several millimetres, are presented in the paper, including PVD and CVD coatings and laser treated surface on the steels and light alloys substrates. The paper also describes the nanostructural effects in solid materials, and especially the counteraction of cracking of new-developed high-manganese austenite steels Fe-Mn-Si-Al by twinning or/and martensitic transformation induced by the cold plastic deformation. The article also outlines the results of research of the development of special micro and nanocomposite materials designed mainly for use in regenerative medicine and regenerative dentistry. The studies of the structure and the properties of newly obtained materials and originally developed technologies are included to present the author’s contribution into materials science, nanotechnology, surface engineering and biomedical engineering including the usefulness of the newly developed nanoengineering materials and their applicability, in particular, in regenerative medicine, as well as tissue engineering. The described outcomes of the research constitute a basis for creating, apart from rigid porous implant-scaffolds, an innovative generation of rigid and elastic biological-engineering composite materials for regenerative medicine. Design/methodology/approach: The article discusses the key aspects of own research performed over the last decade in scope of nanotechnologies, modern biomedical materials and rapid manufacturing techniques used for the fabrication of, in particular, microporous materials applied for medical and dental purposes. The conditions for the performance of the research according to the scope mentioned were ensured by implementation of investment projects for constructing and equipping research and didactic laboratories in scope of nanotechnology, technologies of material processes and computational materials science, including LANAMATE (2010-2014) and MERMFLEG (2010-2013), and also BIOFARMA (2010-2012). Practical implications: The obtained materials and technologies are of high practical importance, which was confirmed in many cases with the results of laboratory tests and investigations at a semi-technical scale, and in some cases with the initiation of implementation works. The results of research in scope of bioengineering and dental engineering may find their applications in tissue engineering, in bone surgery, for threedimensional tissue scaffolds and in dentistry or oncology, to replace the natural tissue removed because of a cancer with the possibility of applying a therapeutic agent. Originality/value: The present paper is the original report from a personal own research and explains the concept, scope and results of own research of a new obtained microporous and nanostructural materials and coatings, including hybride solid-porous products and newly obtained materials processing and additive technologies. Some of the mentioned research results are protected by patents or patent applications, and many of them were awarded over 60 prizes and medals at international fairs of innovation, invention and rationalisation in many countries.

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Katalizatory otrzymywane z prekursorów hydrotalkitowych : materiały nanostrukturalne dla zielonej chemii

Dziembaj R.

Przemysł Chemiczny

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2003

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T. 82, nr 8-9

691-693