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Considering influence of microstructure morphology of epoxy/glass composite on its behavior under deformation conditions - digital material representation case study

Madej L., Malinowski L., Perzynski K., Mojzeszko M., Wang J., Cios G., Czarnecki D., Bala P.

Archives of Civil and Mechanical Engineering

2019

Vol. 19, no. 4

1304--1315

Digital Material Representation (DMR) concept in application to numerical investigation of the two different types of epoxy/glass composite morphologies under loading conditions is addressed within the paper. First, two algorithms for reconstruction of digital microstruc-tures based on metallography investigations are developed. Then, material properties of the investigated epoxy matrix and glass fillers are evaluated based on an in-situ tensile test as well as nano-indentation, respectively. At this stage a numerical investigation is also extended by series of experimental tensile tests to understand basic mechanisms occurring during deformation of the two different types of glass particles fillers. Finally, an example of practical application of the developed digital microstructure model for multi scale calcula-tions of the epoxy/glass composite under loading is presented.

Manufacturing and Macroscopic Properties of Y2O3 Coating Layer on Ceramic (AlN) Substrate Fabricated by Aerosol Deposition

Wi D.-Y., Ham G.-S., Kim S.-H., Lee K.-A.

Archives of Metallurgy and Materials

2018

Vol. 63, iss. 3

1463--1466

This study attempted to manufacture an Y2O3 ceramic coating layer on a ceramic (AlN) substrate using aerosol deposition (AD) and investigated its macroscopic properties. Pure Y2O3 powder with a polygonal shape and average size of 5.0 μm was used as initial feedstock. Using aerosol deposition with suitable process conditions, an Y2O3 coating layer was successfully fabricated on aluminum nitride (AIN). The thickness of the manufactured coating layer was approximately 10 mm. The coating layer consisted of Y2O3 phase identical to that in the initial powder, and no additional oxides were identified. In regard to the roughness of the Y2O3 coating layer, the average roughness (Ra) measured 1.32 μm, indicating that the surface roughness was relatively even compared to the initial powder size (5 μm). Mechanical properties of the Y2O3 coating layer were measured using nano indentation equipment, and the indentation modulus of the Y2O3 coating layer fabricated by aerosol deposition measured 136.5 GPa. The interface of the coating layer was observed using TEM, and the deposition mechanism of the Y2O3 coating layer manufactured by aerosol deposition was also discussed.