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EN
The concept of a miniature transmission electron microscope (TEM) on chip is presented. This idea assumes manufacturing of a silicon-glass multilayer device that contains a miniature electron gun, an electron optics column integrated with a high vacuum micropump, and a sample microchamber with a detector. In this article the field emission cathode, utilizing carbon nanotubes (CNT), and an electron optics column with Einzel lens, made of silicon, are both presented. The elements are assembled with the use of a 3D printed polymer holder and tested in a vacuum chamber. Effective emission and focusing of the electron beam have been achieved. This is the first of many elements of the miniature MEMS (Micro-Electro-Mechanical System) transmission electron microscope that must be tested before the whole working system can be manufactured.
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EN
Purpose: was to investigate impact of cold forming and annealing on microstructural and mechanical properties of HSLA steel. Design/methodology/approach: Testing of Nb-V-Ti microalloyed strip steel was based on a combination of cold rolling, recrystallization annealing, mechanical testing, metallography and TEM. Findings: It was confirmed that by a suitable combination of size of previous cold reduction size and parameters of the following annealing it is possible to influence considerably a complex of mechanical properties of particular strips. Strength as well as plastic properties depended on the course of recrystallization and precipitates' coarsening during annealing. Research limitations/implications: The experiment should be supplemented by the more detailed analyses of microstructure. Practical implications: The results may be utilized for optimization of terms of heat treatment in a cold rolling mill, especially in accordance with specific requirements for a relation between plastic and strength properties of the investigated steel. Originality/value: Research possibilities of VSB-TUO in the sphere of cold rolling of Nb-V-Ti HSLA steel were introduced in combination with the complex approach to processing of the obtained results.
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