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Pcl/Chitosan Blended Nanofibrous Tubes Made by Dual Syringe Electrospinning

Hild M., Al Rez M. F., Aibibu D., Toskas G., Cheng T., Laourine E., Cherif C.

Autex Research Journal

2015

Vol. 15, no. 1

54--59

3D tubular scaffolds made from Poly-(Ɛ-caprolactone) (PCL)/chitosan (CS) nanofibres are very promising candidate as vascular grafts in the field of tissue engineering. In this work, the fabrication of PCL/CS-blended nanofibrous tubes with small diameters by electrospinning from separate PCL and CS solutions is studied. The influence of different CS solutions (CS/polyethylene glycol (PEO)/glacial acetic acid (AcOH), CS/trifluoroacetic acid (TFA), CS/ AcOH) on fibre formation and producibility of nanofibrous tubes is investigated. Attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR) is used to verify the presence of CS in the blended samples. Tensile testing and pore size measurements are done to underline the good prerequisites of the fabricated blended PCL/ CS nanofibrous tubes as potential scaffolds for vascular grafts. Tubes fabricated from the combination of PCL and CS dissolved in AcOH possesses properties, which are favourable for future cell culture studies.

Equilibrium and non-equilibrium states in the compatibilization of PS/PB blends by means of styrene-butadiene block copolymers

Hlavatá D., Horák Z., Hromádková J.

Prace Naukowe Instytutu Technologii Organicznej i Tworzyw Sztucznych Politechniki Wrocławskiej. Konferencje

2001

Vol. 50, nr 23

327-330

Localization of styrene-butadiene block copolymers (BC) in both quenched and slowly cooled polystyrene (PS)/polybutadiene (PB) (4/1) blends was studied by means of small-angle X-ray scattering and transmission electron microscopy. Two types of BCs were used: (a) molecular weight of the styrene blocks is 10 000, i.e. below the critical molecular weight of styrene necessary for the entanglement formation (-18 000), (b) molecular weight of the styrene blocks is 40 000, i.e. it sufficiently exceeds this value. It has been shown that both types of the BCs used are in quickly cooled samples moleculary dispersed at the interface with an exception of 40S-60B-40S-60B-40S. In slowly cooled samples with addition of BCs with "short" styrene blocks, these BCs are released from the PS/PB interface, in contrast to the BCs having "long" styrene blocks.