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The Magnetic and Electric Measurements of the Multiferroic PbFe1/2Nb1/2O3 Ceramics Obtained Using Hot Uniaxial Pressure Method

Bochenek D., Skulski R., Niemiec P., Brzezińska D., Rogacki K.

Archives of Metallurgy and Materials

2018

Vol. 63, iss. 3

1243--1247

We present the results of investigations of Pb(Fe1/2Nb1/2)O3 (PFN) ceramic samples obtained using two-step synthesis (i.e. columbite method). For obtained samples complex investigations of microstructure, magnetic and electrophysical properties have been performed at low and at high temperatures. Microstructure is characterized by small grains with high homogeneity and high density (low porosity). Impedance of samples and the phase shift angle have been measured using LCR Meter. Next the AC electric conductivity, dielectric permittivity and loss tangent have been calculated. AC conductivity at frequency 3 Hz was measured in similar way using Quantum Design PPMS System in magnetic fields 1000 Oe and 10000 Oe. At temperature range 240 K - 260 K the anomalies of conductivity are observed. These anomalies depend on measuring cycle (heating, cooling) and magnetic field.