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Biodegradable polymer coatings on Ti6Al7Nb alloy

Szewczenko Janusz, Kajzer Wojciech, Kajzer Anita, Basiaga Marcin, Kaczmarek Marcin, Antonowicz Magdalena, Nowińska Katarzyna, Jaworska Joanna, Jelonek Katarzyna, Kasperczyk Janusz

Acta of Bioengineering and Biomechanics

2019

Vol. 21, no. 4

83--92

The aim of the study was to determine the influence of long term exposure to Ringer’s solution of biodegradable polymer coatings containing an active substance on the Ti6Al7Nb alloy substrate on the physical and chemical properties of the coatings and the degradation process of the metal substrate. The studies used poly(L-lactide-co-trimethylene carbonate) P(L/TMC), poly(L-lactide-co-trimethylene carbonate-glycolide) P(L/TMC/G) and poly(D,L-lactide-glycolide) (PLGA) coatings applied to the anodically oxidized Ti6Al7Nb alloy by means of dipping method (1, 2 and 3 dips). The polymer coatings contained ciprofloxacin. Roughness and wettability tests were carried out on the substrate and polymer coatings, the pitting corrosion resistance of the substrate and samples with polymer coating was determined, the number of metallic ions released to the solution from the coated and uncoated samples was determined as well as the adhesion of polymer coatings. The research was supplemented by microscopic observations. The results of the research indicate different influence of exposure to Ringer’s solution on the physical and chemical properties of biodegradable polymer coatings containing ciprofloxacin and the course of the degradation process of the metal substrate.

Właściwości powłok hydroksyapatytowych modyfikowanych nanocząsteczkami srebra

Miler M., Sulej-Chojnacka J., Borowski J.

Rudy i Metale Nieżelazne Recykling

2015

R. 60, nr 7

309--315

Głównym celem badań było określenie ilości uwalnianych jonów srebra z powłok hydroksyapatytowych modyfikowanych nanocząstkami srebra. Próbki do badań uzyskano poprzez modyfikację powierzchni stopu tytanu Ti6Al4V, polegającą na natryskiwaniu plazmowym hydroksyapatytu i następnie osadzaniu nanocząstek srebra z zawiesiny. Nanocząstki srebra ze względu na swoje silne właściwości bakteriobójcze są jednym z najbardziej obiecujących nanomateriałów w medycynie. Dzięki zastosowaniu nanocząstek srebra możliwe jest osiągnięcie wysokiego działania przeciwdrobnoustrojowego przy jednoczesnym zastosowaniu niskich stężeń srebra. Z uwagi na aktywne oddziaływanie nanocząstek srebra na ludzki organizm podjęto działania mające na celu wyznaczenie ilości uwalnianych jonów z powierzchni, a także określenie przewodnictwa jonowego. Ponadto modyfikowane powłoki hydroksyapatytowe poddano badaniom zwilżalności powierzchni oraz odporności korozyjnej.

The main purpose of this study was to investigate the kinetics of silver ions release process from hydroxyapatite coating modified with silver nanoparticles. Test samples were obtained by modification of surface of the Ti6Al4V titanium alloy, such modification based on plasma spraying of hydroxyapatite and then deposition of silver nanoparticles from the suspension. Silver nanoparticles because of their strong antibacterial properties are one of the most promising nanomaterials in medicine. Thanks to the use of silver nanoparticles, it is possible to achieve a high antimicrobial activity at a low silver concentration. Due to active interaction of silver nanoparticles on the human body a study to designate the amount of ions released from the surface, as well as the determination of ionic conductivity was carried out. Furthermore, the surface wettability and corrosion resistance study of the modified hydroxyapatite coatings was conducted.

Evaluation of resin composites modified with nanogold and nanosilver

Sokołowski J., Szynkowska M. I., Kleczewska J., Kowalski Z., Sobczak-Kupiec A., Pawlaczyk A., Sokołowski K., Łukomska-Szymańska M.

Acta of Bioengineering and Biomechanics

2014

Vol. 16, no. 1

51--61

Silver and gold have been used for centuries as antimicrobial agents. The aim of the study was to investigate diametral tensile strength, microhardness, ion release and light transmission of experimental resin composites. Flowable dental composite SDR (Dentsply, United Kingdom) was modified by nanogold, nanosilver and silica addition. The metal ion release, light transmission study, microhardness, Diametral Tensile Strength were evaluated. The experimental nanosilver-containing composites released significant amounts of Al, Si, Sr and Ba ions up to 30 days, and negligible silver ion amounts. Significant Ag ion release occurred in nanosilver- and nanogoldmodified composite. Resin composites modified with nanogold and nanosilver deposited on silica carrier exhibit lower light transmission and have opaque appearance. All experimental composites exhibited higher microhardness in comparison to non-modified resin composites. Diametral Tensile Strength of the experimental composites was comparable to the control group.