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1
Content available Crystallization of Eutectics in Fe-C-V-Si Alloys
Kawalec M
Archives of Foundry Engineering
|
2014
|
Vol. 14, iss. 1 spec.
143--146
EN
This article addresses the results of microstructural examinations of the volume solidifying Fe–C–V–Si alloys containing carbon in the range of 1.39÷1.76%, vanadium in the range of 6.77÷7.77% and silicon in the range of 0.02÷3.10. The melting charge was Armco iron, ferro-vanadium with 81.7 wt.%V, spectrally pure graphite and technically pure silica. It was shown that with increasing the silicon content, the microstructure of the resulting alloy changing. These changes include both a matrix the shape of the primary carbides and type of crystallizing eutectic. In the studied alloys was observed following eutectic: fibrous (crystallize as non-faceted/ non-faceted eutectic), complex regular (crystallize as faceted/ non-faceted eutectic), spiral (crystallize as faceted/ faceted eutectic). The results illustrated by the images of the microstructures made with an optical microscope and a scanning electron microscope.
2
Content available Modification of the high-alloyed white cast iron microstructure with magnesium master alloy
Kawalec M.
Archives of Foundry Engineering
|
2013
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Vol. 13, iss. 2
71--74
EN
High-vanadium cast iron is the white cast iron in which the regular fibrous \gamma + VC eutectic with the volume fraction of vanadium carbide amounting to about 20% crystallises. This paper presents the results of studies on high-vanadium cast iron subjected to the inoculation treatment with magnesium master alloy. The aim of this operation is to change the morphology of the crystallising VC carbides from the fibrous shape into a spheroidal one. The study also examines the effect of the amount of the introduced inoculant on changes in the morphology of the crystallising VC carbides. To achieve the goals once set, metallographic studies were performed on high-vanadium cast iron of eutectic composition in base state and after the introduction of a variable content of the inoculant. The introduction of magnesium-based master alloy resulted in the expected changes of microstructure. The most beneficial effect was obtained with the introduction of 1.5% of magnesium master alloy, since nearly half of the crystallised vanadium carbides have acquired a spheroidal shape.
3
Content available Alloyed white cast iron with precipitates of spheroidal vanadium carbides VC
Kawalec M., Górny M.
Archives of Foundry Engineering
|
2012
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Vol. 12, iss. 4
95-100
EN
The paper presents the results of tests on the spheroidising treatment of vanadium carbides VC done with magnesium master alloy and mischmetal. It has been proved that the introduction of magnesium master alloy to an Fe-C-V system of eutectic composition made 34% of carbides crystallise in the form of spheroids. Adding mischmetal to the base alloy melt caused 28% of the vanadium carbides crystallise as dendrites. In base alloy without the microstructure-modifying additives, vanadium carbides crystallised in the form of a branched fibrous eutectic skeleton. Testing of mechanical properties has proved that the spheroidising treatment of VC carbides in high-vanadium cast iron increases the tensile strength by about 60% and elongation 14 - 21 times, depending on the type of the spheroidising agent used. Tribological studies have shown that high-vanadium cast iron with eutectic, dendritic and spheroidal carbides has the abrasive wear resistance more than twice as high as the abrasion-resistant cast steel.
4
Content available Abrasive wear resistance of cast iron with precipitates of spheroidal VC carbides
Kawalec M., Olejnik E.
Archives of Foundry Engineering
|
2012
|
Vol. 12, iss. 2
221-226
EN
The paper presents the results of abrasive wear resistance tests carried out on high-vanadium cast iron with spheroidal VC carbides. The cast iron of eutectic composition was subjected to spheroidising treatment using magnesium master alloy. The tribological properties were examined for the base cast iron (W), for the cast iron subjected to spheroidising treatment (S) and for the abrasion-resistant steel (SH). Studies have shown that high-vanadium cast iron with both eutectic carbides and spheroidal carbides has the abrasion resistance twice as high as the abrasion-resistant cast steel. The spheroidisation of VC carbides did not change the abrasion resistance compared to the base high-vanadium grade.
5
Content available Forming of the microstructure in Fe-C-V alloys
Kawalec M., Fraś E.
Metallurgy and Foundry Engineering
|
2011
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Vol. 37, no. 1
17-24
EN
The study presents the results of microstructural examinations of the volume solidifying Fe-C-V alloys containing carbon in the range of 1.45-2.23% and vanadium in the range of 7.33-15.08%. Attention was focussed on near-eutectic alloys. The Fe-C-V eutectic crystallising in these alloys is composed of ferrite and vanadium carbides of VC1-x type, and as such is included in the group of fibrous eutectics. During research, the experimental eutectic lines were plotted for Fe-C-V alloys, and a formula enabling calculation of the eutectic saturation ratio of these alloys was proposed.
PL
W pracy przedstawiono wyniki badań mikrostruktury stopów Fe-C-V, o zawartości węgla w zakresie 1,45-2,23% i wanadu w zakresie 7,33-15,08%, krystalizujących w sposób objętościowy, przy czym szczególną uwagę zwrócono na stopy okołoeutektyczne. Krystalizująca w stopach Fe-C-V eutektyka składa się z ferrytu i węglików wanadu typu VC1-x i jest zaliczana do grupy eutektyk włóknistych. W pracy określono eksperymentalnie przebieg linii eutektycznej dla stopów Fe-C-V oraz wyznaczono zależność na stopień nasycenia eutektycznego dla tych stopów.
6
Content available The spheroidisation of VC carbides in high-vanadium cast iron
Kawalec M.
Archives of Foundry Engineering
|
2011
|
Vol. 11, iss. 3 spec.
111--116
EN
High-vanadium cast iron is a type of white cast iron, in which a regular fibrous γ + VC eutectic with about 20 vol.% of vanadium carbides crystallises. The paper presents the results of research during which the high-vanadium cast iron was subjected to spheroidisation treatment with magnesium Elmag 5800 master alloy. The purpose of this operation was to obtain the VC carbides of a spheroidal shape. The study also included metallographic examinations and testing of mechanical properties carried out on high-vanadium cast iron of a eutectic composition in as-cast condition and after the spheroidising treatment. The attempt to spheroidise the vanadium carbides has proved to be quite successful. The introduction of magnesium alloy has made nearly one half of the crystallised vanadium carbides acquire a spheroidal shape. The, obtained in this way, high-vanadium cast iron with vanadium carbides of a spheroidal shape showed very high mechanical and plastic properties. The tensile strength Rm increased by 60% compared to the as-cast alloy, while ductility increased more than twenty times. The presented results are based on the initial trials, but further studies of this new material are planned, mainly to check its resistance to abrasion, to impacts and corrosion. Tests are also planned to increase the fraction of spheroidal carbides and measure the effect of their content on the mechanical and tribological properties.
7
Content available remote Microstructure of hypereutectic Fe-C-V alloys
Kawalec M.
Archives of Foundry Engineering
|
2011
|
Vol. 11, iss. 2
55-60
EN
The study shows the results of examinations of the microstructure of the in-volume-solidifying Fe-C-V alloys containing carbon in a range of 1.53-3.09% and vanadium in a range of 14.73-15.71%. All the examined alloys were hypereutectic alloys as proved by the cooling curves, relevant calculations (Sc) and examinations under the microscope. It has been confirmed that the primary carbides of vanadium are crystallising in the form of non-faceted dendrites, acting as a substrate for the growing fibres of vanadium eutectic. The content of primary carbides in the microstructure depends on the content of carbon and vanadium in the alloy. During the conducted research an attempt was also made to determine the content of primary and eutectic carbides and to establish a relationship between carbon and vanadium content in the alloy and the content of primary carbides. In Fe-C-V alloys, besides primary carbides, also a fibrous eutectic composed of ferrite and vanadium carbides of the VC1-x type crystallises. To conduct the previously planned examinations, a series of melts with a variable carbon and vanadium content was carried out under argon atmosphere in a Balzers vacuum furnace. Specimens were examined under an optical microscope, but to investigate in more detail the geometry of individual phases, they were deep etched with aqua regia and examined by scanning electron microscopy. In the investigated alloys, the chemical composition of the crystallised phases was determined by EDS microanalysis.
PL
W pracy przedstawiono wyniki badań mikrostruktury stopów Fe-C-V, o zawartości węgla w zakresie 1.53-3.09% i wanadu w zakresie 14.73-15.71%, krystalizujących w sposób objętościowy. Wszystkie badane stopy są stopami nadeutektycznymi, co potwierdziły krzywe stygnięcia, odpowiednie obliczenia (Sc) oraz obserwacje mikroskopowe. Potwierdzono, że pierwotne węgliki wanadu krystalizują w postaci dendrytów nieścianowych, na których wzrastają włókna eutektyki wanadowej. Udział węglików pierwotnych w mikrostrukturze jest zależny od zawartości węgla i wanadu w stopie. W pracy określono także udział węglików pierwotnych i eutektycznych oraz wyznaczono zależność pomiędzy zawartością węgla i wanadu w stopie a udziałem węglików pierwotnych. Oprócz węglików pierwotnych w stopach Fe-C-V krystalizuje eutektyka włóknista składająca się z ferrytu i węglików wanadu typu VC1-x. W celu wykonania założonych badań przeprowadzono serię wytopów o zmiennej zawartości węgla i wanadu w piecu próżniowym typu Balzers w atmosferze argonu. Próbki obserwowano za pomocą mikroskopu optycznego, a w celu bardziej szczegółowego zbadania geometrii poszczególnych faz trawiono je głęboko wodą królewską i obserwowano za pomocą mikroskopu skaningowego. W badanych stopach przeprowadzono również pomiary składu chemicznego wykrystalizowanych faz metodą punktowej mikroanalizy EDS.
8
Content available remote Shaping of the microstructure in neareutectic Fe-C-V alloys
Kawalec M., Fraś E.
Archives of Foundry Engineering
|
2010
|
Vol. 10, iss. 4
83--88
EN
The study presents the results of microstructural examinations of the volume solidifying Fe-C-V alloys containing carbon in the range of 1.45÷2.23% and vanadium in the range of 7.33÷15.08%. Attention was focussed on near-eutectic alloys. The Fe-C-V eutectic crystallising in these alloys is composed of ferrite and vanadium carbides of VC1-x type, and as such is included in the group of fibrous eutectics. During research, the experimental eutectic lines were plotted for Fe-C-V alloys, and a formula enabling calculation of the eutectic saturation ratio of these alloys was proposed.
9
Content available remote Abrasive wear resistance of high-vanadium cast iron
Kawalec M., Fraś E.
Archives of Foundry Engineering
|
2009
|
Vol. 9, iss. 4
103-108
EN
The study presents the results of tribological tests made on Fe-C-V and Fe-C-V-Si alloys undergoing volume solidification and containing carbon in a range of 1,43-2,58%, vanadium in a range of 5,34-14,77%, and silicon in a range of 1,06-3,69%. The, crystallising in Fe-C-V alloys, eutectic is composed of ferrite and vanadium carbides of the VC1-x type, and as such is included in the group of fibrous eutectics. Introducing silicon additions to the Fe-C-V system changes the geometry of the crystallising eutectic from fibrous into complex regular, while the shape of the primary carbides crystallising as non-faceted-non-faceted dendrites changes into a faceted form. It has been proved that the type of matrix has also a very important effect on the abrasive wear behaviour. The possibility has been indicated to manufacture Fe-C-V alloys with matrix containing lamellar pearlite, characterised by the abrasive wear resistance comparable to that of Hadfield cast steel. It is also possible to make alloys which will have the matrix composed of a mixture of lamellar and granular pearlite, or of a mixture of lamellar pearlite and cementite, and in this case their abrasive wear resistance will be superior to that of Hadfield cast steel. Within the examined range of chemical compositions, the addition of silicon has been reported to reduce the abrasive wear resistance.
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