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The high-pressure sorptomat - a novel apparatus for volumetric sorption studies under isobaric high gas pressure conditions

Kudasik Mateusz, Anioł Łukasz, Skoczylas Norbert

Metrology and Measurement Systems

2022

Vol. 29, nr 4

607--620

As part of the work the high-pressure sorptomat - a novel apparatus for sorption tests under conditions of high gas pressure was developed. The sorption measurement is carried out using the volumetric method, and the precise gas flow pressure regulator is used in the device to ensure isobaric conditions and regulate the sorption pressure in the range of 0-10 MPa. The uniqueness and high precision of sorption measurements with the constructed apparatus are ensured by the parallel use of many pressure sensors with a wide measurement range as well as high precision of measurement - due to the use of precise pressure sensors. The obtained results showed, i.a. that the time of reaching the isobaric conditions of the measurement is about 6-7 seconds and it is so short that it can be considered a quasi-step initiation of sorption processes. Moreover, the results of the measurement pressure stabilization tests, during the CO2 sorption test on activated carbon, have shown that the built-in pressure regulator works correctly and ensures isobaric sorption measurement conditions with the precision of pressure stabilization of ±1% of the measurement pressure. The maximum range of sorption measurement using the high-pressure sorptomat is 0-86 400 cm3/g, and the maximum measurement uncertainty is ±2% of the measured value. The activated carbon sample used for the tests was characterized by a high sorption capacity, reaching 104.4 cm3/g at a CO2 pressure of 1.0 MPa.