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Open porosity of cement pastes and their gas permeability

Tracz T.

Bulletin of the Polish Academy of Sciences. Technical Sciences

2016

Vol. 64, nr 4

775--783

This paper presents the results of extensive research work on the open porosity and gas permeability of cement pastes. Tests were conducted on cement pastes with different water/cement ratios and types of cement. The three most popular cements in Poland from the CEM I, CEM II and CEM III groups were tested after the pastes had been cured for 90 days in laboratory conditions. The scope of experiments included the assessment of open porosity determined using three different methods: comparing the bulk and specific densities, mercury intrusion porosimetry and saturating the material with water. In addition, this article contains an analysis of the porosity characteristics based on the distributions produced by porosimetry examinations. Gas permeability was determined using the modified RILEM-Cembureau laboratory method. The results of the completed test allowed a quantitative determination to be made of the impact of water-cement ratio and type of cement used on open porosity assessed by various methods, and the influence of these parameters on the gas permeability of the paste. The quantitative changes in the content of capillary pores and meso-pores in the cement pastes analysed are also presented.

Helium porosity measurements for rocks from unconventional reservoirs performed on crushed samples

Klaja J., Łykowska G., Przelaskowska A.

Nafta-Gaz

2015

R. 71, nr 11

856--863

Porosity measurements for rocks from unconventional reservoirs pose a challenge due to their extremely low permeability, small pore dimensions, and high content of organic matter and clay minerals. The presented work was aimed at adapting the helium porosity measurement methodology for the investigation of microporous rocks. The carried out studies have shown that the measurement conditions are important, which applies both to the measurement pressure and the grain size. The highest porosity values were obtained for measurements performed on samples crushed to grain size < 0.5 mm.

Pomiary porowatości skał ze złóż niekonwencjonalnych stanowią wyzwanie ze względu na bardzo niską przepuszczalność, niewielkie rozmiary porów, wysoką zawartość substancji organicznej i minerałów ilastych. Przedstawiona praca ma na celu przystosowanie metodyki pomiaru porowatości helowej do badań skał mikroporowych. Wykonane badania wykazały, że warunki pomiaru mają tutaj duże znaczenie, dotyczy to zarówno ciśnienia pomiaru i rozmiaru ziaren. Najwyższe wartości porowatości uzyskano dla pomiarów wykonanych na próbkach pokruszonych do frakcji < 0,5 mm.