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Influence of heat treatment on changes on structure and magnetic properties of CoSiB alloy

Nowosielski R., Zajdel A., Lesz S., Kostrubiec B., Stokłosa Z.

Journal of Achievements in Materials and Manufacturing Engineering

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2008

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Vol. 27, nr 2

147-150

EN

Purpose: This paper describes influence of heat treatment on changes on structure and magnetic properties of the amorphous Co77Si11.5B11.5 alloy. Design/methodology/approach: The following experimental techniques were used: X-ray diffraction (XRD), static and dynamic measurements of magnetic properties (magnetic balance, fluxmeter, Maxwell-Wien bridge). Findings: The crystallization process involved by heat treatment leads to significant changes of structure and magnetic properties of amorphous Co77Si11.5B11.5 alloy. Research limitations/implications: Practical implications: The attractive properties of Co-Si-B alloy are of special interest for basic research on the materials as well as for their potential applications, like magnetic sensors. According to the results presented in this paper the examined Co77Si11.5B11.5 alloy as a soft magnetic material may be used in noise filters, saturable reactors, miniature inductance elements for abating spike noise, zero-phase current transformers, and magnetic heads etc., i.e. devices which are expected to exhibit high levels of permeability at high frequencies. Originality/value: It has been shown that thermal annealing at temperature close to the crystallization temperature leads to a significant increase of the initial magnetic permeability.

2

Crystallization of amorphous Co77Si11.5B11.5 alloy

Nowosielski R., Zajdel A., Lesz S., Kostrubiec B., Stokłosa Z.

Archives of Materials Science and Engineering

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2007

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Vol. 28, nr 3

141-148

EN

Purpose: The investigation results of crystallization of amorphous Co77Si11.5B11.5 alloy in tape form, obtained by melt spinning method during annealing in temperature range 373-873 K with step of 50 K in time 1 h, have been presented in the paper. Design/methodology/approach: The following experimental techniques were used: X-ray diffraction (XRD), electrical resistivity in situ measurements (four-point probe) static and dynamic measurements of magnetic properties (magnetic balance, fluxmeter, Maxwell-Wien bridge). Findings: The changes of magnetic properties connected with the structure changes involved by crystallization process have been investigated of amorphous Co77Si11.5B11.5 alloy. Practical implications: Amorphous magnetic materials have been around for some time and their applications can be found in many types of industrial products. They include transformers, motors, and a wide variety of magnetic components in sensors, power electronics, electrical energy control/management systems, telecommunication equipment and pulse power devices. Originality/value: It has been stated that heat treatment leads to crystallization leads to a significant increase of the initial magnetic permeability.

3

Crystallization kinetics of an amorphous Co77Si11.5B11.5 alloy

Nowosielski R., Zajdel A., Lesz S., Kostrubiec B., Stokłosa Z.

Journal of Achievements in Materials and Manufacturing Engineering

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2006

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Vol. 17, nr 1-2

121--124

EN

Purpose: This paper describes crystallization kinetics and changes magnetic properties involved by process of crystallization Co-Si-B amorphous alloy. Design/methodology/approach: The following experimental techniques were used: X-ray diffraction (XRD), electrical resistivity in situ measurements (four-point probe) static and dynamic measurements of magnetic properties (magnetic balance, fluxmeter, Maxwell-Wien bridge). Findings: In this work has been performed influence of thermal annealing on crystallization kinetics and magnetic properties amorphous Co77Si11.5B11.5 alloy. Practical implications: The attractive properties of Co-Si-B alloy are of special interest for basic research on the materials as well as for their potential applications, like magnetic sensors. The Co soft magnetic material is used in noise filters, saturable reactors, miniature inductance elements for abating spike noise, mains transformers, choke coils, zero-phase current transformers, and magnetic heads etc., i.e., devices which are expected to exhibit high levels of permeability at high frequencies. Originality/value: It has been shown that thermal annealing at temperature close to the crystallization temperature leads to a significant increase of the initial magnetic permeability.

4

Crystallisation kinetics and magnetic properties of a Co-based amorphous alloy

Lesz S., Nowosielski R., Kostrubiec B., Stokłosa Z.

Journal of Achievements in Materials and Manufacturing Engineering

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2006

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Vol. 16, nr 1-2

35--39

EN

Purpose: In the present paper, the kinetics of crystallization process and its correlation with magnetic properties of the Co80Si9B11 alloy was carefully examined. Design/methodology/approach: The following experimental techniques were used: X-ray diffraction (XRD), electrical resistivity in situ measurements (four-point probe), saturation magnetization in situ measurements (magnetic balance) and initial relative magnetic permeability measurements (Maxwell-Wien bridge). Findings: The investigations proved that thermal annealing of amorphous Co80Si9B11 alloy leads to a crystallization process and radical changes of magnetic properties. The activation energy of this process was determined as Ec=3.0±0.2 eV. Research limitations/implications: According to the results presented in the present paper the examined alloys can be used as a very good soft magnetic material. Originality/value: The best soft magnetic properties are observed in as quenched state.