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3 2013

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The MFM studies of the surface domain structure of Sm–Fe–Co–Zr–Cu thin ribbons

Dośpiał M., Nabiałek M., Szota M., Michta Ł., Wieczorek P., Błoch K., Pietrusiewicz P., Oźga K., Michalczyk J.

Optica Applicata

2013

Vol. 43, nr 1

195--200

The article contains studies of micro- and domain structures obtained using atomic/magnetic force microscopy (AFM/MFM) of melt-spun Sm12.5Fe8Co65.5Zr1Cu13 thin ribbons in the as-cast state. In order to obtain the SmCo8.5 type of structure in the Sm–Fe–Co–Zr–Cu alloy, thin ribbons were manufactured using the melt-spinning method with large linear velocity of a copper wheel and proper selection of alloying elements. The obtained samples in the as-cast state were magnetized. The microscopic results were also supported by magnetic measurements performed on a vibrating sample magnetometer as well as by a quantitative analysis of phase composition obtained using the Rietveld refinement method.

Magnetic properties and surface domain structure of (Nd0.85Dy0.15)10Fe83Zr1B6 thin ribbons

Ceglarek A, Plusa D, Dospial M, Nabialek M, Wieczorek P

Optica Applicata

2013

Vol. 43, nr 1

117--122

In this paper, the nanocrystalline (Nd0.85Dy0.15)10Fe83Zr1B6 ribbons produced by melt-spinning have been investigated by the X-ray diffraction method (XRD), vibrating sample magnetometer (VSM) and magnetic force microscopy (MFM). The XRD studies showed that material investigated was mainly composed of Re2Fe14B and α-Fe phases with fine grain sizes of 25 and 9 nm, respectively. The magnetic parameters determined from the hysteresis loop measurements are as follows: μ0HC = 0.96 T, μ0MR = 0.76 T, μ0MS = 1.09 T, (BH)max = 88 kJ/m3. The large remanence ratio (μ0MR/μ0MS) of 0.7 results from the exchange coupling between the soft and hard magnetic grains. The large surface interaction domains revealed by MFM confirmed the existence of strong exchange coupling between nanosize grains.

Structural and magnetic properties of the as - cast Nd10Fe83Zr1B6 ribbons, studied by X-ray diffraction and Mössbauer spectroscopy

Ceglarek A., Płusa D., Pawlik P., Gębara P.

Nukleonika

2013

Vol. 58, No. 1

105-108

The Nd10Fe83Zr1B6 alloy ribbons, prepared by melt-spinning technique, have been investigated by X-ray diffraction (XRD) and Mossbauer spectroscopy. Magnetic properties were studied by Faraday balance and vibrating sample magnetometry (VSM). The ribbon samples were produced at various surface velocities of the copper wheel from 10 m/s to 20 m/s. The XRD and Mossbauer spectra analysis have shown that the ribbons consist of the soft magnetic alfa-Fe, hard magnetic Nd2Fe14B and disordered phases. The results showed that a uniform Nd2Fe14B/alfa-Fe nanocomposite structure with fine alfa-Fe grains can be obtained at an optimum velocity of the cooper roll of 20 m/s. The samples produced in these conditions had the best magnetic properties (mi0HC= 0.84 T, mi0MR = 1.05 T, mi0MS = 1.36 T, (BH)max = 160 kJ/m3) with strong exchange coupling between the hard magnetic Nd2Fe14B and soft magnetic mi-Fe phases. The amorphous phase existing between grains causes an increase in the remanence and remanence ratio.