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Parametric optimisation of microhardness on heat-treated electroless Ni-YSZ cermet coating

Bahiyah Baba N., Ghazali A. S., Abdul Rahman A. H., Sharif S

Journal of Achievements in Materials and Manufacturing Engineering

2022

Vol. 112, nr 1

33--41

Purpose: The paper discusses the parametric optimisation of the electroless Ni-YSZ cermet coating microhardness upon heat treatment. Heat treatment is a process to increase the mechanical properties of the electroless nickel coating and it can be enhanced by manipulating its parameters. Parametric optimisation is conducted by the design of experiment full factorial 3x3 with 27 runs. Treating temperature, treating time and ceramic particle size parameters at 3-level are evaluated using statistical tool ANOVA in Minitab20. Design/methodology/approach: Ni-YSZ cermet coating is deposited onto a high-speed steel substrate using the electroless nickel co-deposition method. The temperature and time were varied in a range of 300-400°C and 0-2 hours respectively. The microhardness measurements were carried out using a Vickers microhardness tester (Shimadzu) according to ISO 6507-4. The surface characterisation was analysed using Cambridge Stereoscan 90 Scanning Electron Microscope (SEM) coupled with Energy Dispersive X-ray Analysis (EDXA). Findings: The optimum condition in obtaining high microhardness on Ni-YSZ cermet coating is evaluated by statistical tool ANOVA in Minitab20 software. It is found that the most significant parameter for high microhardness is at the treating temperature of 400°C followed by treating time at 2 hours using nano-sized YSZ particles. The ceramic particle size is found not a significant parameter in obtaining a high microhardness, however it has effect on interaction between treating temperature and treating time. Research limitations/implications: The paper only limits to the optimisation condition of microhardness on Ni-YSZ cermet coating hardness property by varying heat treatment parameters. Practical implications: The optimisation condition obtained might only applicable to the electroless Ni-YSZ cermet coating with similar electroless nickel solution and treatments. Originality/value: The value of this work is the heat treatment parametric optimisation to obtain high microhardness on electroless Ni-YSZ cermet coating by using the design of experiment 3-level full factorial.

Critical evaluation into the practical utility of the Design of Experiments

Sharma Mithun, Sharma Shilpi

Engineering Management in Production and Services

2021

Vol. 13, no. 3

50--65

The research aims to emphasise the relevance of the Design of Experiments (DOE) technique as a reliable method for ensuring efficient use of statistical methods in routine industrial processes. A case study approach with a deductive strategy was used to assess the effectiveness of different DOE methods to achieve the desired objectives. Screening, mid-resolution and high-resolution DOE methods helped identify, characterise, and optimise an experimental variable against the desired output response. A general framework for effective DOE is provided as part of DOE planning, including defining DOE objectives, selection criteria, noise reduction, and application across industries. Overall, various DOE models proved successful in identifying a complicated relationship between experimental variables and output response. However, when ideal DOE models may not be feasible, reducing test run by choosing lower resolution DOE or fewer replicates can still provide important insights into the experimental variables’ impact on output responses.