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New application of 1,1,3,3,3-Pentafluoropropene-diethylamine Adduct (PFPDEA) as Fluorinating Agent. Synthesis of 3,3,3-Trifluoropropionates of Vicinal Fluorohydrins

Walkowiak J., Haufe G., Koroniak H.

Polish Journal of Chemistry

2004

Vol. 78 / nr 9

1777-1784

Reaction of various omega-fluoro-(omega-1)-hydroxy and omega-hydroxy-(omega-1)-fluoro fatty acid methyl esters with adduct of 1,1,3,3,3-pentafluoropropene-diethylamine (PFPDEA) has been studied. As a products mixture of corresponding vicinal difluorides and vicinal fluoro-3,3,3-trifluoropropionates was obtained.