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Post-Synthesis Microwave Plasma Treatment Effect on Magnetization and Morphology of Manganese-Iron Oxide Nanoparticles

Busharat Muhammad Aqib, Naz Muhammad Yasin, Shukrullah Shazia, Zahid Muhammad

Archives of Metallurgy and Materials

2022

Vol. 67, iss. 3

837--842

The influence of microwave (MW) plasma on magnetization and morphology of sol-gel synthesized MnFe2O4 ferrite nanoparticles is investigated in this study. Manganese (II) nitrate hexahydrate, ferric (III) nitrate nanohydrate and citric acid were used to synthesize ferrite nanoparticles via a facile sol-gel route. These ferrite nanostructures were heat-treated at 700ºC and then given MW plasma treatment for 10 min. The pristine MnFe2O4 and plasma treated MnFe2O4 showed almost similar structural formation with a slight increase in crystallinity on plasma treatment. However, XRD peak intensity slightly increased after plasma treatment, reflecting better crystallinity of the nanostructures. The size of the particle increased from 35 nm to 39 nm on plasma treatment. It was challenging to deduce the surface morphology of the nanoparticles since both samples were composed of a mixture of big and small clusters. Clusters that had been treated with plasma were larger in size than pristine ones. The band gap energy of the pristine MnFe2O4 sample was about 5.92 eV, which increased to 6.01 eV after treatment with MW plasma. The saturation magnetization of MnFe2O4 sample was noted about 0.78 emu/g before plasma treatment and 0.68 emu/g after MW plasma treatment.

Preparation and microwave absorption of M type ferrite nanoparticle composites

Shen G. Z., Cheng G. S., Cao Y., Xu Z.

Materials Science Poland

2010

Vol. 28, No. 1

327--334

The sol-gel method was used to obtain M type BaFe12O19 ferrite nanoparticles. Rod like and flake like ferrite nanoparticles can be successfully fabricated by controlling the heating process of the precursor. The phase attributes, morphology and grain size of BaFe12O19 ferrite were characterized by TEM and XRD. The complex permittivity and permeability of ferrite epoxy resin composites were measured in the Ku waveband (12.4-18 GHz). Ferrite composites containing short carbon fibres have also been fabricated in order to obtain higher complex permittivities of the composites. The reflectivities of these ferrite composites were calculated according to the measured electromagnetic parameters. The results show that the microwave absorption properties of ferrite composites can be effectively improved by filling them with short carbon fibres.