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Wpływ zawartości grafitu na właściwości mechaniczne warstw hybrydowych Ni-P/Si3N4/grafit osadzonych na stopie AW-7075 metodą redukcji chemicznej

Czapczyk Kazimierz

Przemysł Chemiczny

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2024

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T. 103, nr 1

86--92

PL

Przedstawiono wpływ obecności grafitu jako fazy dyspersyjnej na właściwości mechaniczne warstw hybrydowych Ni-P/Si₃N₄/grafit, które osadzono metodą redukcji chemicznej na stopie glinu AW-7075. Wykonano badania morfologii powierzchni warstw metodą mikroskopii świetlnej i skaningowej. Dalszą część pracy stanowiły badania mechaniczne, czyli pomiary mikrotwardości warstw oraz ich adhezji do aluminiowego podłoża, a także analizy wpływu obecności grafitu na podstawowe właściwości materiału powłokowego. Zbadano próbki ze stopu AW-7075, na których osadzono metodą bezprądową powłoki hybrydowe i porównawczo nanokompozytowe o różnym składzie chemicznym, modyfikowanym zawartością faz dyspersyjnych.

EN

The mech. and adhesive properties of Ni-P/Si₃N₄ and Ni-P/Si₃N₄/graphite coatings deposited using the electroless method on the AW-7075 Al alloy were compared. Coatings with different chem. compns., modified by the content of dispersion phases (Si₃N₄ and graphite), were used. Microhardness and adhesion of the layers to the Al substrate were measured. The impact of the presence of graphite on the basic properties of the coating material was analyzed. The surface morphol. of the layers was examined using light microscopy and SEM. The incorporation of Si₃N₄ and graphite into the coating material resulted in a several-fold increase in the microhardness of the surface layer compared to the Al alloy.

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Effect of particle size on surface roughness and morphology of heat-treated electroless Ni-YSZ coating

Bahiyah Baba N., Ghazali A. S., Azinee S. N., Abdul Rahman A. H., Sharif S.

Journal of Achievements in Materials and Manufacturing Engineering

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2022

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Vol. 114, nr 1

5--14

EN

Purpose: The paper discusses the surface characterisation of electroless nickel-yttria-stabilised zirconia (Ni-YSZ) coating with varying YSZ particle sizes and undergoes heat treatment at a temperature between 300-400°C for 1-2 hours for wear resistance purposes. This finding will be helpful to the application of Ni-YSZ as an alternative coating for cutting tools. Design/methodology/approach: The surface characterisation was analysed using JOEL Scanning Electron Microscope (SEM) coupled with Energy Dispersive X-ray (EDX) JSM 7800F. The crystallographic structure of materials was analysed by X-ray diffraction (XRD) Bruker D8 Advance instrument. The Ni-YSZ coating was deposited using electroless nickel co-deposition of 8YSZ ceramic particles with a nano, mixed and microparticle sizes onto a high-speed steel (HSS) substrate. The coatings were heat treated at temperature 300-400°C and time 1-2 hours. The surface roughness was measured using Mitutoyo surface roughness tester SJ-301. Findings: The electroless Ni-YSZ coating deposited has an average thickness of 30 μm. It is found that the coating morphology electroless coating without YSZ particle incorporation (EN) and Ni-YSZ nano (N) is smoother compared to the Ni-YSZ mixed (NM) and Ni-YSZ micro (M). The EDS composition analysis shows the YSZ content in the electroless Ni-YSZ coating for N samples is the lowest, whereas NM samples are the highest. This resulted in the surface roughness behaviour where the mixed-size YSZ particle gives the highest roughness at all temperatures. The XRD analysis shows that heating temperatures above 300°C caused the precipitation of Ni3P crystalline. Research limitations/implications: Previous studies in the surface characterisation of electroless nickel composite are scarce; thus, the study has limitations in finding supporting data. Originality/value: The surface characterisation especially related to the surface roughness of the electroless nickel, either the Ni-P or composites or alloys are rarely reported. Thus, this study enlightened the effect of particle size on surface roughness and morphology of heat-treated coatings.

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Electroless Deposition of Composite Nickel-Phosphorous Coatings with Diamond Dispersoid

Petrova M., Georgieva M., Chakarova V., Dobreva E.

Archives of Metallurgy and Materials

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2016

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Vol. 61, iss. 2A

493--498

EN

The composite Ni-P coating with diamond particles (D) deposited on the flexible substrates of pressed polyethylene terephthalate material (PET) was obtained, to be used in the development of efficient, flexible grinding and polishing tools. The optimal conditions of the hydrodynamic regime, deposition time and temperature were found. The influence of the concentration and size of the D particles (3/7 ÷ 225/300 μm) on the coating thickness and number of co-deposited particles were studied. By Scanning Electron Microscopy (SEM) images were defined the morphology of dispersion coatings and number of co-deposited particles in them, and Energy Dispersive Spectroscopy (EDS/INCA) was used to determine the elemental chemical composition of the composite coatings.