This paper presents the results of the determination of the structure of diphase media, namely the emulsion of transformer oil in water. The determination was made by solving the so-called inverse problem. The necessary information about the medium was gained using the attenuation spectra analysis. Research was limited to the attenuation spectra measurements and multiple repeated modeling. The results were compared with the measured spectra. The knowledge regarding the optical properties of phases of the emulsion was necessary hi these calculations. The spectra of refraction indexes of oil and water as well as the spectrum of attenuation coefficient were measured.
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