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Study of Si morphology in AlSi21CuNiMg cast alloy using col our and deep etching

Tillová Eva, Chalupová Mária, Kuchariková Lenka, Bonek Mirosław, Uhríčik Milan, Pastierovičová Lucia

Bulletin of the Polish Academy of Sciences. Technical Sciences

2023

Vol. 71, nr 2

art. no. e144618

The effect of possible modification and refining effect of Al-Cu-P-based pre-alloy combined with Fe on the microstructure and the silicon morphology change in hypereutectic Al-Si cast alloy was studied. The samples in the as-cast state were observed by optical and scanning electron microscopy with energy-dispersive X-ray spectroscopy. The 3D morphology of both primary and eutectic silicon was observed by using colour and deep etching in detail. The results showed that the AlCu19P1.4 pre-alloy (1.07 wt.%) combined with the addition of Fe (0.02 wt.%) has a significant effect on the change of the amount, size and morphology of primary Si. This is significantly refined and changes the shape from a coarse irregular star-shaped, polyhedral, or plate-like shape to a fine polyhedral shape. The average size of the primary Si is reduced by about of 78 % from 135 μm to 28 μm and the number of primary Si particles increased from 7.4 to 237. No change in the morphology of the eutectic Si was observed; a refinement of the structure from a coarse needle/plate-like to a fine plate-like structure was seen. The depth etching method using HCl was very effective in the study of the 3D silicon morphology observed, which could be observed in detail without the presence of artefacts.

Pomiary naprężeń własnych tytanu Ti6Al4V po procesach kulowania na potrzeby inżynierii biomedycznej

Bańczerowski Jakub, Mońka Grzegorz, Skalski Konstanty

Inżynieria Powierzchni

2019

nr 4

10--17

W pracy przedstawiono wyniki pomiarów naprężeń własnych odpowiednio przygotowanych próbek tytanu Grade 5 (Ti6Al4V). Próbki były uprzednio kulowane śrutem stalowym o średnicach 0,6 mm, i 1,2 mm i twardości 640 HV. Przeprowadzono pomiary naprężeń własnych metodą Waismana-Philipsa polegającą na pomiarze strzałki ugięcia próbki w próbie trawienia stopu tytanu Ti6Al4V w roztworze kwasu fluorowodorowego (HF) i siarkowego (H2SO4). Badanie przeprowadzono na stanowisku zaprojektowanym i wykonanym wcześniej w Instytucie Mechaniki Precyzyjnej (IMP). W celu oceny wpływu parametrów procesu kulowania na próbki wykonano pomiary chropowatości ich powierzchni przed trawieniem. Wyznaczenie wartości i rozkładów naprężeń własnych sprowadza się, jak nadmieniono, do określenia zmian krzywizny w funkcji zmian grubości badanej próbki, a następnie wykonaniu niezbędnych obliczeń. Wyniki pomiaru przemieszczeń w funkcji czasu oraz grubości próbek uzyskane po trawieniu posłużyły do wyznaczenia wartości naprężeń własnych w funkcji odległości od powierzchni próbki. Obliczenia wykonano przy pomocy programu NWW 11.

The paper presents results of measurements of residual stresses of the properly prepared Grade 5 titanium (Ti6Al4V) samples. The samples previously underwent the process of shot-peening with steel shots with 0.6 mm, and 1.2 mm in diameter and 640 HV hardness. Measurements of residual stresses were carried out using the Waismman-Philips method consisting in measuring the sample deflection arrow in the etching test of Ti6Al4V titanium alloy in the solution of hydrofluoric acid (HF) and sulfuric acid (H2SO4). Tests were carried out on the stand designed and constructed earlier at the Institute of Precision Mechanics (IMP). In order to assess the impact of the shot-peening process parameters on the samples, roughness measurements of the surface before etching were carried out. Determining the values and distributions of the residual stresses is reduced, as mentioned, to determining the changes in curvature as a function of changes in the thickness of the sample tested, and then conducting the necessary calculations. The results of the measurement of displacements as a function of time and thickness of the samples obtained after etching were used to determine the value of residual stresses as a function of distance from the sample surface. Calculations were conducted with using the NWW.11 program.

Using Deep Etching in the Study of Eutectic Silicon 3D-Morphology in AlSi7MgTi Cast Alloy

Kuchariková L., Tillová E., Bonek M. S., Chalupová M.

Archives of Metallurgy and Materials

2018

Vol. 63, iss. 4

2017--2022

The effect of combination grain refinement with AlTi5B1 master (55 ppm) and Sr-modification with AlSr5 master (20, 30, 40, 50 and 60 ppm) on the microstructure, tensile and hardness properties of AlSi7MgTi cast alloy were systematically investigated. Eutectic silicon was studied by optical and scanning electron microscopy after standard (0.5% HF) and deep etching (HCl). Morphology of eutectic Si changes from compact plate-like (as-cast state) to fibbers (after modification). Si-fibbers in samples with 50 and 60 ppm Sr coarsen probably as a result of over-modification. The optimum mechanical properties has the experimental material which was grain refined and modified with 40 ppm of Sr (UTS = 220.6 MPa; ductility = 6.1%, and 82.3 HBW 5/250/15).