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Carbonization of solid uranyl-ascorbate gel as an indirect step of uranium carbide synthesis

Brykala M., Rogowski M., Olczak T.

Nukleonika

2015

Vol. 60, No. 4, part 2

921--925

The studies of the synthesis of uranium carbide from uranyl-ascorbate gels using the complex sol-gel process (CSGP) have been carried out. The synthesis of uranyl-ascorbate mixture as liquid sol from uranium trioxide and ascorbic acid and solid gel by extraction of water from sol were carefully examined. Ascorbic acid was used as a complexing agent in complex sol-gel process and as a carbon source. The crucial step to obtain final uranium carbides from the aforementioned substrates is the carbonization process. The thermal behavior of ascorbic acid and uranyl-ascorbate gels in a nitrogen atmosphere in the temperature range of 25–900°C were investigated using TG-DTG. Furthermore, the products of the carbonization of uranyl-ascorbate gels in nitrogen, argon and vacuum atmosphere were identifi ed by X-ray diffraction. TG-DTG was used also as a method for determining of carbon residues in the samples.