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Crystallization, the cast structure and the formation of gas blowholes in high-nitrogen steels and alloy steels.

Svyazhin A.G., Siwka J., Skuza Z., Prokoshkina V.G., Kaputkina L.M.

Inżynieria Materiałowa

2001

R. XXII, nr 5

884-887

In the paper, the results of experimental research concerning the precipitation of nitrogen in the form of gas blowholes during the crystallization of supersaturated Fe-N, Fe-O-S-N alloys and 1Cr13 and Cr18Ni10 steels have been described. It has been found that the precipitation of nitrogen gas blowholes is more intensive and the pressure pN2 is higher at low contents of surface active elements, i.e. oxygen and sulphur. At the concentration ([%O] + 0.5%[%S]) > or = 300 ppm, microingots exhibited a compact macrostructure without gas blowholes. The results of a kinetic analysis of the process of desorption of nitrogen and the thermodynamics of the investigated solution (including surface tension) confirm that the surface reaction plays a decisive role in the formation of gas blowholes. For this reason, it is possible to eliminate the formation of gas blowholes in ingots of ferritic and ferritic-austenitic steels by introducing such SAE admixtures, as Sb, Te or Se. Analytical expressions have been obtained, which define the amount of nitrogen releasing into gas blowholes and describe the conditions for producing ingots or casting of a compact structure at cooling rates of approximately 10 to the 3 K/s.