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1 Materials Science Poland

1 2010

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On the design of biodegradable hydrogels both thermosensitive and pH sensitive

Wang B., Guo Y., Hu G.

Materials Science Poland

2010

Vol. 28, No. 1

207--215

A Pluronic oligo(?-caprolactone) block copolymer has been synthesized by ring opening polymerization of ?-caprolactone monomers in the presence of poly(ethylene oxide)-poly(propylene oxide) -poly(ethylene oxide) triblock copolymers, using stannous octoate as a catalyst, and then the block copolymer was terminated with an acryloyl group. A novel biodegradable pH- and temperature sensitive hydrogel has been fabricated by free radical copolymerization of diacylated macromer-methacrylic acid aqueous solution initiated by a redox initiator. The structures of products were characterized by the Fourier transform infrared spectroscopy. Variations of the equilibrium swelling ratio in various environmental solutions confirmed the pH- and temperature sensitivity of hydrogel, which were affected by the MAA content.