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Crown Ethers with Azo or Azoxy Unit and Sulfur Atom(s) in 16-Membered Macrocycle

Szczygelska-Tao J., Kravtsov V. Ch., Biernat J. F.

Polish Journal of Chemistry

2001

Vol. 75, nr 7

991-1000

16-membered crown ethers bearing oxygen and sulfur atom(s) and an azo or azoxy group in the macrocycle have been synthesized by reductive macrocyclization of respective dinitropodands. Behavior of the compounds as ionophores in ion-selective membrane electrodes has been studied. The structure of 16-membered azothiacrown ether has been solved by X-ray analysis.