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2 Archives of Metallurgy and Materials

2 2023

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Synthesis of Ti-Nb-Zr Alloys Combined Powder Metallurgy and Arc Melting Methods

Matuła Izabela, Dercz Grzegorz, Prusik Krystian, Szklarska Magdalena, Kazek-Kęsik Alicja, Simka Wojciech, Sudoł E.

Archives of Metallurgy and Materials

2023

Vol. 68, iss. 3

1115--1120

Scientists and medics are still searching for new metallic materials that can be used in medicine, e.g., as material for implants. The following article proposes materials based on titanium with vital elements prepared by combined powder metallurgy and arc melting methods. Four compositions of Ti-28Ta-9Nb, Ti-28Ta-19Nb, Ti-28Ta-9Zr and Ti-28Ta-19Zr (wt.%) have been prepared. The tested material was thoroughly analyzed by X-ray diffraction and scanning electron microscopy. Qualitative phase analysis using X-ray diffraction showed the presence of two phases, α' and β titanium. In addition, a microhardness test was conducted, and the material was characterized in terms of corrosion properties. It was found that the corrosion resistance decreases with an increase of the β phase presence.

Effect of Nb and Zr alloying additives on structure and properties of Ti-Ta-Nb-Zr alloys for medical applications

Dercz Grzegorz, Matuła Izabela, Prusik Krystian, Zając J., Szklarska Magdalena, Kazek-Kęsik Alicja, Simka Wojciech

Archives of Metallurgy and Materials

2023

Vol. 68, iss. 3

1137--1142

This work investigated two titanium-based alloys with a constant tantalum content and variable contents of alloy additives - niobium and zirconium. The Ti-30Ta-10Zr-20Nb (wt.%) and Ti-30Ta-20Zr-10Nb (wt.%) alloys were obtained using a combination of powder metallurgy and arc melting methods. The influence of alloying additives on the structure and properties of the Ti-Ta-Nb-Zr system was studied using, among others: X-ray diffraction and scanning electron microscopy. The X-ray diffraction confirmed the single-β-phase structure of both alloys. In addition, the microscopic analysis revealed that a higher amount of zirconium favoured the formation of larger grains. However, the microhardness analysis indicated that the alloy with the higher niobium content had the higher microhardness. Importantly, the in vitro corrosion study revealed that the addition of niobium promoted the better corrosion resistance of the investigated alloy.