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2 Archives of Metallurgy and Materials

2 2018

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The Effect of Atomic Layer Deposition of ZrO2 on the Physicochemical Properties of Cobalt based Alloys Intended for Prosthetic Dentistry

Ziębowicz A., Woźniak A., Ziębowicz B., Kosiel K., Chladek G.

Archives of Metallurgy and Materials

2018

Vol. 63, iss. 3

1077--1082

The paper presents the effect of ZrO2 layer deposition by the ALD process on the physicochemical properties of cobalt-based alloys (Realloy C and EOS CoCr SP2) intended for application in prosthetic dentistry. The paper shows the results of the surface roughness measurements made by the AFM method as well as the wettability and free surface energy measurements. Additionally, potentiodynamic tests of pitting corrosion resistance and electrochemical impedance spectroscopy in a solution of artificial saliva were carried out. Tests were carried out on the samples in the initial state and after surface modification with the ZrO2 layer. Based on these results, the usefulness (e.g. enhancement of corrosion resistance and biocompatibility) of the proposed ZrO2 layer on the cobalt alloys was assessed.

Physicochemical Properties of Oxide ZrO2 Layer Deposited by Sol-Gel Method on Ti-6Al-7Nb Alloy

Woźniak A., Ziębowicz B., Ziębowicz A., Walke W.

Archives of Metallurgy and Materials

2018

Vol. 63, iss. 3

1209--1215

The paper contains the results of the initial surface treatment influence on the properties of the medical Ti-6Al-7Nb alloy with a modified zirconium oxide layer deposited on its surface by sol-gel method. In the paper, the analysis of results of potentiodynamic studies is presented as well as its resistance to pitting corrosion and electrochemical impedance spectroscopy (EIS), macroscopic observation of the surface of samples and analysis of geometrical structure with the use Atomic Force Microscope (AFM) were performed. The studies were performed on two groups of samples depending on the graduation of the sand used in sandblasted process – 50 μm and 250 μm. Based on the obtained results it can be concluded that the type of the initial surface treatment preceding the surface modification of the Ti-6Al-7Nb has a significant effect on its properties.