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Investigation of Bio-Functional Properties of Titanium Substrates After Hybrid Oxidation

Jasinski J. J.

Archives of Metallurgy and Materials

2020

Vol. 65, iss. 1

141--149

In order to enhance bioactive properties of titanium 99.2 used in implantology and various biomedical applications, numerous methods to form tight oxide coatings are being investigated. Some of these interesting techniques for generating TiO2 coatings include: electrochemical methods with anodizing, electric discharge treatment, plasma methods (PVD) and diffusive methods (i.e. oxidation in a fluidized bed). Each method aims to create a thin homogenous oxide coating characterized with thermal stability and repassivation ability in the presence of body fluid environment. However, new methods are still sought for increasing the biocompatibility of the substrate following a change in the intensity of depositing on the oxide coating compounds with high biocompatibility with body tissues, including hydroxyapatite, which constitutes the basis for subsequent osseointegration processes. The article presents investigation of HAp formation on titanium substrate surface after hybrid oxidation process. Hybrid surface treatments combine methods of fluidized bed atmospheric diffusive treatment FADT with the PVD surface treatment realized with different parameters (FADT - 640°C / 8h and PVD - magnetron sputtering with TiO2 target). In order to investigate the effects of hybrid oxidation and the formation of HAp molecules, SEM-EDS, SEM-EBSD, STEM-EDS, RS, nanoindentation and Kokubo bioactivity tests (c-SBF2) were carried out. The hybrid method of titanium oxidation, proposed by the Author, presents a new outlook on themodification and development of the properties of oxide coatings in the area of biomedical applications. Combining the ways of Ti Grade 2 oxidation in the hybrid method highly improves the formation of hydroxyapatite compounds and shows the potential of applying such a technique in implantology, where the intensive growth of bone tissues is crucial.

An influence of Titanium Alloy Ti10V2Fe3Al Microstructure on the Electrodischarge Process Efficiency

Żyra A., Bogucki R., Skoczypiec S.

Archives of Metallurgy and Materials

2019

Vol. 64, iss. 3

1005--1010

In the work results of research on electrodischarge machining (EDM) of titanium alloy Ti10V2Fe3Al with (α + β) structure were presented. Preliminary heat treatment of samples allows to obtain different morphology and volume fraction of the α phase. The main goal of research was to assessment of the material microstructure impact on EDM technological factors (ie. material removal rate, tool wear) and morphology of technological surface layer. Electrodischarge machining is alternative and increasingly used method of titanium alloys machining. Research allowed to indicate the possibilities and limitations of use EDM in this area. It is especially important in the aspect of parts produced for aircraft industry and related requirements for the technological surface layer quality.