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Thermogravimetric analysis of modified cellulose mixtures in air

Zawieja Z., Sawicki J.

Archives of Metallurgy and Materials

2019

Vol. 64, iss. 1

153--157

The paper includes the TG-DTG thermogravimetric air-testing of a cellulose mixture modified with the additives of expanded vermiculite or expanded perlite. A thermal degradation test was carried out at 1000°C with a simultaneous qualitative analysis of the emitted gases. During the thermal degradation process, the thermal effects were also measured. The research results indicate that expanded vermiculite or expanded perlite do not emit toxic gases during thermal degradation. The cellulose mixture modification, with the additives of expanded vermiculite or perlite, does not result in the creation of new gaseous compounds in the process of thermal degradation. As investigated below, the mixtures tested in this article find application in gating systems for supplying liquid metal in no-bake moulds. Such cellulose-based material solutions shall allow the foundry industry to introduce less gas vaporising technologies within the entire casting production process.

The novel metal complexes with ketoprofen. thermal and spectroscopy investigations

Gacki M., Kafarska K.

Acta Innovations

2017

no. 25

47--56

The novel metal complexes of ketoprofen (Hket)(1) with general formulae Mn(L)4(2), Co(L)4(3), Ni(L)4(4), and Zn(L)4(5) (where L= Hket, ket) were synthesized and characterized by elemental analysis, FTIR- spectroscopy and thermal decomposition techniques. All IR spectra revealed absorption bands related to the asymmetric (νas) and symmetric (νs) vibrations of carboxylate group. The Nakammoto criteria clearly indicate that this group is bonded in a bidentate-chelate mode. The thermal behavior of complexes was studied by TG, DTG methods under dynamic condition in air. Upon heating, all compounds decompose progressively to metal oxides, which are the final products of pyrolysis.