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1 Polish Journal of Chemistry

1 2009

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Synthesis of New Type of Macrocyclic Lactones Functionalized with Different Groups and Investigation of Their Metal Binding Abilities

Ertul S., Bayrakci M.

Polish Journal of Chemistry

2009

Vol. 83, nr 3

493-502

New type of macrocyclic lactones functionalized with different groups were synthesized by reaction of the dihydroxy compounds such as 5a-d with suitable glycolyl chloride such as tri, tetra dicarboxylic acid dichloride derivatives. Their metal complexes with NaClO4źH2O, KClO4 and Ba(ClO4)2źH2O were studied. Furthermore, their metal-pic rate extraction studies with metal salts such as Na+, K+, Cu2+, Ni2+ and Hg2+ from aqueous phase to organic phase were attempted. All the structures of the ligands and complexes were confirmed by 1H-, 13C-NMR, IR, UV-Vis, MS and elemental analyses methods.