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Structure of the S304H Steel after 20,000 Hours of Ageing

Wersta Robert, Zieliński Adam, Sroka Marek, Puszczało Tomasz, Sówka Karol

Archives of Metallurgy and Materials

2022

Vol. 67, iss. 2

487--493

The S304H steel is used in the construction of pressure components of boilers with supercritical operating parameters. The paper presents the results of the research on the microstructure after ageing for 20,000 hours at 650 and 700°C. The microstructure examination was performed using scanning and transmission electron microscopy. The precipitates were identifies using transmission electron microscopy. The influence of ageing time on microstructure changes and the precipitation process of the tested steel is described. The presented research results are an element of material characteristics of the new generation of steel, which are used in the design work of pressure devices of steam boilers and in diagnostic work during operation.

Analysis of the precipitation process of secondary phases after long-term ageing of the S304H steel

Zieliński Adam, Wersta Robert, Sroka Marek

Bulletin of the Polish Academy of Sciences. Technical Sciences

2021

Vol. 69, nr 5

art. no. e137520

S304H steel is used in the construction of pressure components of boilers with supercritical operating parameters. The paper presents the results of research on the microstructure following ageing for 30,000 hours at 650 and 700°C. Microstructure examination was performed using scanning and transmission electron microscopy. The precipitates were identified using transmission electron microscopy. The paper analyses the precipitation process and its dynamics depending on the temperature and ageing time in detail. MX carbonitrides and the ε_Cu phase were proved to be the most stable phase, regardless of the test temperature. It was also showed that the M₂₃C₆ carbide precipitates in the tested steel and the intermetallic sigma phase (σ) may play a significant role in the loss of durability of the tested steel. This is related to their significant increase due to the influence of elevated temperature, and their coagulation and coalescence dynamics strongly depend on the ageing/operating temperature level. The qualitative and quantitative identification of the secondary phase precipitation processes described in the study is important in the analysis of the loss of durability of the tested steel under creep conditions.