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The GdF3/MgF2 bilayer as an antireflective narrow-band ultraviolet filter

Marszałek K., Małek A., Winkowski P.

Optica Applicata

2016

Vol. 46, nr 2

187--197

The effective work of optical systems, applied in advanced optic and optoelectronic devices, requires antireflective coatings. In this work we focus on designing the bilayer system dedicated to work as a narrow-band filter within UV range of electromagnetic spectrum. Such coatings are applied in lasers where reduction in reflection to a small value at any single wavelength is needed. The bilayer system is based on GdF3 and MgF2 used as materials with middle and low refractive index. The multilayers were obtained by thermal evaporation on a highly purified CaF2 substrates. The spectral dispersion of the refractive index of single layers has been determined by ellipsometric measurements. Thicknesses of single layers included in the bilayer system, aimed to work at specific wavelength, have been optimized based on optical characteristics simulation, including experimentally measured values of the refractive indices. During the deposition, layer thickness and deposition rate were controlled with Inficon XTC/2 thickness measuring system. Optical properties of obtained GdF3/MgF2 bilayer systems have been determined based on spectral dependences of reflectance and transmittance measured with the application of a spectrophotometer. The crystal structure and phase composition of the films have been examined by X-ray diffraction. The result of studies revealed that proper optimization of thicknesses of individual layers creating GdF3/MgF2 bilayer systems makes it possible to obtain the antireflective coating for desired wavelength of electromagnetic spectrum. The GdF3/MgF2 antireflective bilayer will be applied as a narrow-band filter for 238 nm irradiation produced by gas-ion/BBO crystal laser.

Szkło-ceramika tlenkowo-fluorkowa z fazą GdF3

Środa M., Sitarz M., Szlósarczyk K.

Materiały Ceramiczne

2012

T. 64, nr 2

272-276

W pracy przedstawiono badania nad otrzymaniem szkieł tlenkowo-fluorkowych wykazujących zdolność do tworzenia się niskofononowych faz opartych na GdF3, jako przezroczystych materiałów szklano-krystalicznych dla optoelektroniki. Szkła otrzymano w układzie SiO2-Al2O3-Na2F2-Na2O-GdF3. Ich skład był modyfikowany tlenkami B2O3, BaO i MgO. Przeprowadzone badania pokazały, że tworzenie fazy GdF3 w szkłach krzemianowo-glinowych jest utrudnione. Poprzez odpowiedni dobór modyfikatorów (wprowadzenie B2O3 lub BaO) jest jednak możliwe otrzymanie niskofononowej fazy w oparciu o dwuskładnikowe fluorki, np. NaGdF4 i BaGdF5.

Glass-ceramics with the low phonon phases of fluorides as a transparent materials for optoelectronic application were studied. Glasses based on the SiO2-Al2O3-Na2F2-Na2O-GdF3 system was obtained. Their chemical composition was modified with B2O3, BaO or MgO. The study shows that formation of GdF3 is much more difficult than LaF3 from alumino-silicate glasses. It is possible to induce the formation of low phonon phases NaGdF4 and BaGdF5 at the first stage of crystallization when B2O3 or BaO are the components of the glass.