Wyniki wyszukiwania - BazTech

1

Structural characterization of low-carbon multiphase steels merging advanced research methods with light optical microscopy

Radwański K.

Archives of Civil and Mechanical Engineering

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2016

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Vol. 16, no. 3

282--293

EN

The paper presents new approach to characterizing low-carbon multiphase steels structure by means of concurrent application of optical and scanning electron microscopy with the emphasis on the latter one. Limitations of optical microscopy in material structure analysis, and the possibilities of information interchange between both methods have been discussed. The microstructure characterization is mostly based on the results obtained by means of scanning electron microscopy with wide application of EBSD method. As part of the work, fundamental constituents of multiphase steels structure with particular focus on consideration of the possibility of influencing their morphological features during thermal treatment have been systematized and described. Referring to the sheets of TRIP 700 and DP 600 steel, a capability of combining the FEG SEM analysis with EBSD method to characterize their structure was presented. EBSD method enables not only distinction of phases of various crystalline structure. Owing to analysis of parameters such as IQ, FIT, CI, KAM and misorientation angle, it is possible to differentiate constituents having different crystal structure. The method of IQ distribution curve deconvolution allows estimation of the fraction of structure constituents representing the same crystal structure. Existence of characteristic ranges of misorientation angles for selected structure constituents was proven.

2

Analiza zmian struktury stopów z układu Fe-Al po procesie walcowania na gorąco

Bednarczyk I., Jabłońska M., Hyrcza-Michalska M.

Hutnik, Wiadomości Hutnicze

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2014

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Vol. 81, nr 8

513--518

PL

W pracy analizowano wyniki badań zmian struktury stopów z układu Fe-Al po procesie walcowania na gorąco. Badanie struktury wyjściowej (przed odkształceniem) oraz ewolucja struktury odkształconych stopów z układu Fe-Al określona została m.in. metodą wysokorozdzielczej skaningowej mikroskopii elektronowej sprzężonej z techniką EBSD oraz metodą skaningowej transmisyjnej mikroskopii elektronowej. Zastosowanie mikroskopii wysokorozdzielczej SEM i techniki EBSD pozwoliło na określenie opisu struktury badanych stopów jaki towarzyszy odkształceniu plastycznemu na gorąco.

EN

The paper presents the results of the structure changes analysis of alloys from Fe-Al system after the hot rolling process. Investigating the initial structure before deformation and the evolution of the structure of the hot deformed alloys was determined, inter alia, with high resolution scanning electron microscopy coupled EBSD technique by scanning and transmission electron microscopy. Use of the high resolution SEM microscopy and EBSD techniques allowed to provide additional information regarding the description of the structure tested alloys that accompany hot plastic deformation.

3

EBSD Strain Analysis of CuZn10 Cast Alloy During Cavitational Wear

Jasionowski R., Zasada D., Polkowski W.

Archives of Foundry Engineering

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2013

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Vol. 13, iss. 1 spec.

51--56

EN

Microstreams of liquid formed during the implosion of cavitation bubbles and the effects of pressure waves coming from disappearing bubbles are the main causes of damage of the washed surface, leading to loss of material (the cavitation erosion). Repeated cavitation implosions cause non-uniform stress state resulting in the strengthening of the surface layer, change of micro-geometry and surface cracks leading to detachment of the material particles. Course of cavitation erosion process depends on the effects of plastic deformation at the beginning of the destruction. The aim of this study was analysis of plastic deformation by EBSD method of CuZn10 cast alloy at the beginning of the cavitation destruction process.

4

Grain size reduction in the 713C nickel superalloy as a result of heat treatment

Lachowicz M. B., Faryna M., Podrez-Radziszewska M.

Archives of Foundry Engineering

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2011

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Vol. 11, iss. 2 spec.

143--148

EN

The paper presents metallographic test results for the 713C nickel superalloy after heat treatment and crystallographic orientation analysis performed with the EBSD method. The 713C alloy was subjected to annealing in the temperature of 950 ºC for 30 hours followed by aircooling. As a result of the applied heat treatment the local grain size reduction in the alloy was observed. It has been found that in the primary grains the new subgrains of different crystallographic orientation are created. Between the new grains and the primary grains the boundaries of high angle appear. Orientation change in the micro-areas is closely related to the carbides rebuilding and volume diffusion of elements dissolved in the γ - γ’ alloy matrix and the (NbTi)C carbides.

5

Nowe możliwości badania struktury materiałów metodą dyfrakcji elektronów wstecznie rozproszonych

Piątkowski A.

LAB Laboratoria, Aparatura, Badania

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2005

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R. 10, nr 4

21-24

6

Identyfikacja faz metodą EBSD - problemy preparatyki

Klimek L., Jakubowski K.

Inżynieria Materiałowa

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2003

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R. XXIV, nr 6

318-321

PL

Identyfikacja faz metodą dyfrakcji elektronów wstecznie rozproszonych ma potencjalnie szerokie zastosowanie w inżynierii materiałowej. Mimo, że jest to metoda stosunkowo prosta to jednak otrzymywane linie dyfrakcyjne nie zawsze są prawidłowo detektowane przez komputer. Przyczyny tego tkwią najczęściej w preparatyce próbek. W pracy przedstawiono wpływ sposobu w jaki zostały przygotowane zgłady metalograficzne wybranych materiałów na jakość otrzymywanych obrazów dyfrakcyjnych, a tym samym na możliwości identyfikacji obserwowanych faz. Przeprowadzone badania wykazały, że sposób przygotowania zgładów metalograficznych w bardzo dużym stopniu wpływa na identyfikację faz. Przy czym trudno jest ustalić uniwersalną preparatykę dla wszystkich materiałów.

EN

Electron back scattered diffraction method of phases identification potentially has broad application in the materials science. Despite the fact that this method is relatively simple, obtained diffraction lines are not always correctly identified by a computer. Purposes of this are - in most cases - because of the samples preparation. The influence of the metallographic specimens preparation method of chosen materials on the quality of EBSP and on the possibility of phases identification has been presented in this work. During the research it was shown that the method of metallographic specimens preparation influences significantly the phases identification. In the mean time is very difficult to state the universal method of preparation for all the materials.