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1 Polish Journal of Chemistry

1 2006

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The Synthesis and Characterization of (1Z,2Z)-N~1~,N~2~Dihydroxy-N~1~,N~2~ dipyridin-2-ylethanedimidamide and Its Mono and Dinuclear Zn(II), Cd(II) and Hg(II) Complexes

Kakanejadifard A., Niknam E.

Polish Journal of Chemistry

2006

Vol. 80, nr 10

1651-1656

The novel Schiff base ligand, 4-methoxysalicyliden-p-aminoacetophenoneoxime (LH) was synthesized starting from p-aminoacetophenoneoxime and 4-methoxysalicylaldehyde. Mononuclear cobalt(II), copper(II) and zinc(II) complexes of the ligand have been prepared by using Co(II), Cu(II) and Zn(II) salt with a metal to ligand ratio of 1:2. The structures of the ligand and its complexes were identified by using elemental analyses, IR, 1H- and 13C-NMR spectra, magnetic susceptibility measurements, UV spectra and thermogravimetric analyses (TGA).