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2 2015

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Ti6Al4V porous elements coated by polymeric surface layer for biomedical applications

Dobrzański L. A., Dobrzańska-Danikiewicz A. D., Gaweł T. G.

Journal of Achievements in Materials and Manufacturing Engineering

2015

Vol. 71, nr 2

53--59

Purpose: The aim of the paper is to characterise titanium alloy Ti6Al4V coated by polymeric surface layer as a material for biomedical applications. The paper presents a Selective Laser Melting (SLM) method of fabrication of elements to be used as implants from Ti6Al4V powder. It was demonstrated that the metallic scaffolds created have strictly defined geometric dimensions of an object and open pores, and the pores are regular and repeat within the whole volume of the biomimetic element. Design/methodology/approach: The actual manufacturing process is preceded with creating a model of an element in the stl format that allows to present the element surface by means of a net of triangles. Once the shape is defined of a unit cell and its net parameters, i.e. height, depth and width, they are duplicated with appropriate mathematical algorithms as a result of which a strictly defined, densed and complicated structure of pores defined by a designer is created. Findings: Scanning electron microscopy was applied for showing the structure of pure scaffolds as well as composites made of Ti6Al4V scaffolds coated by polymeric surface layer. Microscope observations were performed using a SEM Zeiss Supra 35 equipped with EDS detectors for chemical composition analysis. Practical implications: Manufactured metal-polymer composites can be used in regenerative medicine as biomimetic implants. Originality/value: The characteristics of biomimetic composites, used in medicine as implants of a palate piece loss with strictly designed geometric shape and dimensions of the object and its strictly planed pores.

Fabrication Of Scaffolds From Ti6Al4V Powders Using The Computer Aided Laser Method

Dobrzański L. A., Dobrzańska-Danikiewicz A. D., Malara P., Gaweł T. G., Dobrzański L. B., Achtelik-Franczak A.

Archives of Metallurgy and Materials

2015

Vol. 60, iss. 2A

1065--1070

The aim of the research, the results of which are presented in the paper, is to fabricate, by Selective Laser Melting (SLM), a metallic scaffold with Ti6Al4V powder based on a virtual model corresponding to the actual loss of a patient’s craniofacial bone. A plaster cast was made for a patient with a palate recess, and the cast was then scanned with a 3D scanner to create a virtual 3D model of a palate recess, according to which a 3D model of a solid implant was created using specialist software. The virtual 3D solid implant model was converted into a 3D porous implant model after designing an individual shape of the unit cell conditioning the size and three-dimensional shape of the scaffold pores by multiplication of unit cells. The data concerning a virtual 3D porous implant model was transferred into a selective laser melting (SLM) device and a metallic scaffold was produced from Ti6Al4V powder with this machine, which was subjected to surface treatment by chemical etching. An object with certain initially adopted assumptions, i.e. shape and geometric dimensions, was finally achieved, which perfectly matches the patient bone recesses. The scaffold created was subjected to micro-and spectroscopic examinations.

Celem badań, których wyniki zaprezentowano w artykule jest wytworzenie, metodą selektywnego topienia laserowego (SLM), scaffoldu metalowego z proszku Ti6Al4V na podstawie wirtualnego modelu odpowiadającego rzeczywistemu ubytkowi kości twarzoczaszki pacjenta. Od pacjenta z ubytkiem podniebienia pobierano wycisk gipsowy, który następnie zeskanowano za pomocą skanera 3D, w celu uzyskania wirtualnego modelu 3D ubytku podniebienia, na podstawie którego z użyciem specjalistycznego oprogramowania utworzono model 3D litego implantu. Po zaprojektowaniu indywidualnego kształtu komórki jednostkowej, determinującej wielkość i trójwymiarowy kształt porów scaffoldu, poprzez multiplikację komórek jednostkowych przekształcono wirtualny model 3D implantu litego w model 3D implantu porowatego. Dane dotyczące wirtualnego modelu 3D implantu porowatego przetransferowano do urządzenia służącego do selektywnego topienia laserowego (SLM) i z użyciem tej maszyny z proszku Ti6Al4V wytworzono metalowy scaffold, który poddano obróbce powierzchniowej poprzez trawienie chemiczne. Finalnie otrzymano obiekt o założonych na wstępie: kształcie i wymiarach geometrycznych, które idealnie odpowiadają ubytkowi kości pacjenta. Wytworzony scaffold poddano badaniom mikro i spektroskopowym.