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1 2018

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Method of utilization of the spent vanadium catalyst

Mazurek K., Grzesiak P., Drużyński S., Kiełkowska U., Wróbel A., Szalla A.

Polish Journal of Chemical Technology

2018

Vol. 20, nr 3

1--7

A spent vanadium catalyst, from the plant of metallurgical type, was leached in a potassium hydroxide solution to recover vanadium. The effect of time, temperature, concentration of basic, catalyst particle size and phase ratio was studied. The results showed that for a 160–750 μm catalyst leached for 4 h at 313.15 K in the presence of 10% potassium hydroxide solution at a liquid: solid ratio of 20:1, the extent of leaching of V was about 87%. Additionally, separation of vanadium from such a solution was investigated by the ion exchange method. Two types of polymer strongly basic ion exchangers were used. The ion exchange tests indicate that vanadium were loaded from the post-leaching solution with high efficiency. On this basis a flowsheet for the proposed process of a complex utilization of the spent vanadium catalyst is presented.