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Sequential recovery processes of tungsten from hubnerite mineral concentrate of Qash Amir mineralized quartz veins, South Eastern Desert, Egypt

Abu Khoziem Hanaa Abdelaal

Physicochemical Problems of Mineral Processing

2021

Vol. 57, iss. 5

91--105

A hubnerite (MnWO4) mineral concentrate was prepared from the mineralized quartz veins of Gabal Qash Amir muscovite granite. This W- concentrate was chemically processed to obtain the more economic highly pure tungsten oxide. To accomplish this goal, two successive atmospheric agitation leaching processes were conducted. The first includes HCl acid agitation leaching to breakdown hubnerite mineral structure. The purpose was also to get rid of the associated Mn and Fe contents from one hand, and to prepare the more important intermediate tungstic acid from the other hand. From the latter, a sodium tungstate (Na2HWO4) leach liquor was adequately prepared after applying the second atmospheric NaOH agitation leeching process using the optimum conditions of 40% caustic soda concentration at solid/ liquid ratio of 1/3, 180oC for 2h. Finally, 7% Alamine 336 in kerosene was used for extracting 93.7% of W content under the studied optimum conditions of O/A ratio of 1/1, contact time 7 min at room temperature (20±5oC) and pH of 8.

Equilibrium and rate of iron(III) extraction from chloride solutions by individual hydrophobic extractants and their mixtures

Staszak K., Cierpiszewski R., Prochaska K.

Polish Journal of Chemical Technology

2011

Vol. 13, nr 1

1-5

The main goal of this work was to study and compare the rate of iron(III) extraction from chloride solutions by commercial extractants: Alamine 336, TOPO and LIX 54 and their mixtures. Using the interfacial tension data, obtained for mixed systems, the values of surface mole fraction and molecular interaction parameter of extractants were estimated. Determination of the extraction rates was performed by using the Lewis-type stirred transfer cell. It was found that the extraction efficiency of extractants are changed in the following order: Alamine 336>TOPO>β-diketone. The addition of a chelating extractant to the system decreases the extraction efficiency, for example the addition of β-diketone to TOPO decreases the extraction efficiency by about 50%.