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Effect of Variable Manganese Content on Microstructure of Al-Cu Alloys

Stąpór S., Górny M., Kawalec M., Gracz B.

Archives of Metallurgy and Materials

2020

Vol. 65, iss. 4

1377--1383

The presented access the influence of Mn content (0-0.94 wt.%) on the course of the cooling curves, phase transformation, macrostructure, and microstructure of Al-Cu alloys for three series: initial (Series I), with the addition of an AlTi master (Series II), and modified with AlTi5B1 (Series III). The maximum degree of undercooling ΔT was determined based on the cooling curves. The surface density of the grains (NA ) was determined and associated with the inverse of solidification interval 1/ΔTk . Titanium (contained in the charge materials as well as the modifier) has a significant effect on the grinding of the primary grains in the tested alloys. A DSC thermal analysis allowed for the determination of phase transition temperatures under conditions close to equilibrium. For series II and III, the number of grains decreases above 0.2 wt.% Mn with a simultaneous increase in solidification interval 1/ΔT2 . The presence of Al2 Cu eutectics as well as the Cu-, Fe-, and Mn-containing phases in the examined samples was demonstrated using scanning electron microscopy.

The Effect of Nickel on Shaping the Structure of Al-Cu-Mn Alloys

Górny M., Sikora G., Tyrała E.

Journal of Casting & Materials Engineering

2017

Vol. 1, no. 1

20--26

This study investigated the effect of nickel on shaping the structure of aluminum alloys of the Al-Cu-Mn type in the “as-cast” condition and after heat treatment according to the T6 procedure. The aluminum alloys of type Al-5%Cu-1%Mn, containing nickel in a range of up to 1.9%, were taken into consideration in this work. Experiments were carried out for thin-walled thickness casting (g = 5 mm) and for reference casting with a wall thickness of g = 35 mm. Metallographic investigations of both the macro- and micro-structure were conducted to estimate the secondary dendrite arm spacing (SDAS), average diameter (dav) of the primary α (Al) grains, and surface fraction of the interdendritic phases (f). Moreover, the degree of dissolution of these interdendritic phases during the solution treatment process was determined. An SEM-EDS analysis was conducted, from which it follows that the addition of nickel at the level of 0.5% changes the un-dissolved particles from a needle-like β-Fe shape to blocky and coagulated. Higher additions of nickel starting from 0.88%) give rise to as many as four phases with higher copper content, the deficit of which results in the smaller strengthening effect of α (Al) dendrites.